tert-butyl (R)-3-(benzyloxycarbonylamino)-4-(3,4-dimethoxyphenyl)butanoate

Base Information

Chemical Name:tert-butyl (R)-3-(benzyloxycarbonylamino)-4-(3,4-dimethoxyphenyl)butanoate
CAS No.:1258740-20-3
Molecular Formula:C₂₄H₃₁NO₆
Molecular Weight:429.513
Hs Code.:

Synonyms:tert-butyl (R)-3-(benzyloxycarbonylamino)-4-(3,4-dimethoxyphenyl)butanoate

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Chemical Property of tert-butyl (R)-3-(benzyloxycarbonylamino)-4-(3,4-dimethoxyphenyl)butanoate

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Technology Process of tert-butyl (R)-3-(benzyloxycarbonylamino)-4-(3,4-dimethoxyphenyl)butanoate

There total 1 articles about tert-butyl (R)-3-(benzyloxycarbonylamino)-4-(3,4-dimethoxyphenyl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.0%

: 89980-69-8
3,4-dimethoxyphenylmagnesium bromide

: 668475-45-4
(2R)-2-tert-butoxycarbonylmethyl-aziridine-1-carboxylic acid benzyl ester

: 1258740-20-3
tert-butyl (R)-3-(benzyloxycarbonylamino)-4-(3,4-dimethoxyphenyl)butanoate

: 100-51-6,185532-71-2
benzyl alcohol

Guidance literature:: 3,4-dimethoxyphenylmagnesium bromide; (2R)-2-tert-butoxycarbonylmethyl-aziridine-1-carboxylic acid benzyl ester; With copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; at -40 - 0 ℃; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; at 0 ℃; regioselective reaction;
DOI:10.1016/j.tet.2010.09.025