α-methyl-9-phenanthrylacetonitrile

Base Information

• Chemical Name: α-methyl-9-phenanthrylacetonitrile
• CAS No.: 128479-21-0
• Molecular Formula: C₁₇H₁₃N
• Molecular Weight: 231.297
• Mol file: 128479-21-0.mol

Synonyms:α-methyl-9-phenanthrylacetonitrile

Chemical Property of α-methyl-9-phenanthrylacetonitrile

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α-methyl-9-phenanthrylacetonitrile

There total 2 articles about α-methyl-9-phenanthrylacetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

9-bromophenanthrene (573-17-1) + propiononitrile (107-12-0) → 9-Aminophenanthrene (947-73-9) + α-methyl-9-phenanthrylacetonitrile (128479-21-0)

Guidance literature:

With ammonia; sodium; iron(III) chloride; In 1,4-dioxane; for 0.5h;

DOI:10.1055/s-1994-25613

Reference yield: 27.0%

9-bromophenanthrene (573-17-1) → 9-Aminophenanthrene (947-73-9) + α-methyl-9-phenanthrylacetonitrile (128479-21-0)

Guidance literature:

With ammonia; sodium; iron(III) chloride; propiononitrile; In 1,4-dioxane; for 0.5h;

DOI:10.1055/s-1994-25613

Reference yield: 78.0%

α-methyl-9-phenanthrylacetonitrile (128479-21-0) → 2-(9-phenanthryl)propanoic acid (128479-27-6,130060-20-7,40452-19-5)

Guidance literature:

With sulfuric acid; In water; acetic acid; for 2h; Heating;

DOI:10.1002/ardp.19903230412

upstream raw materials:

9-bromophenanthrene

propiononitrile

Downstream raw materials:

2-(9-phenanthryl)propanoic acid