(3-hydroxy-[1,1'-biphenyl]-4-yl)(phenyl)methanone

Base Information

Chemical Name:(3-hydroxy-[1,1'-biphenyl]-4-yl)(phenyl)methanone
CAS No.:51531-18-1
Molecular Formula:C₁₉H₁₄O₂
Molecular Weight:274.319
Hs Code.:

Synonyms:(3-hydroxy-[1,1'-biphenyl]-4-yl)(phenyl)methanone

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Chemical Property of (3-hydroxy-[1,1'-biphenyl]-4-yl)(phenyl)methanone

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Technology Process of (3-hydroxy-[1,1'-biphenyl]-4-yl)(phenyl)methanone

There total 4 articles about (3-hydroxy-[1,1'-biphenyl]-4-yl)(phenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: C₁₄H₁₃NO₂

: 611-73-4
Benzoylformic acid

: 51531-18-1
(3-hydroxy-[1,1'-biphenyl]-4-yl)(phenyl)methanone

Guidance literature:: With dipotassium peroxodisulfate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate; silver carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 24h; Sealed tube;
DOI:10.1002/ejoc.201900242

Reference yield:

: 1079392-34-9
C₂₀H₁₃NO₃

: 51531-18-1
(3-hydroxy-[1,1'-biphenyl]-4-yl)(phenyl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / methanol; chloroform / 1 h / 20 °C

2: sodium carbonate / ethyl acetate; water / 2 h / 0 °C / Sealed tube

3: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver carbonate; dipotassium peroxodisulfate; cesium acetate / N,N-dimethyl-formamide / 24 h / 120 °C / Sealed tube

With dipotassium peroxodisulfate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate; sodium carbonate; hydrazine hydrate; silver carbonate; In methanol; chloroform; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201900242

Reference yield:

: 5122-95-2
3-Biphenylboronic acid

: 51531-18-1
(3-hydroxy-[1,1'-biphenyl]-4-yl)(phenyl)methanone

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) chloride; pyridine / 1,2-dichloro-ethane / 20 °C / Molecular sieve

2: hydrazine hydrate / methanol; chloroform / 1 h / 20 °C

3: sodium carbonate / ethyl acetate; water / 2 h / 0 °C / Sealed tube

4: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver carbonate; dipotassium peroxodisulfate; cesium acetate / N,N-dimethyl-formamide / 24 h / 120 °C / Sealed tube

With pyridine; dipotassium peroxodisulfate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate; sodium carbonate; hydrazine hydrate; silver carbonate; copper(l) chloride; In methanol; chloroform; water; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201900242