(E)-2-(3-(4-(1H-1,2,4-triazole-1-yl)styryl)-5,5-dimethylcyclohex-2-enylidene)malononitrile

Base Information

• Chemical Name: (E)-2-(3-(4-(1H-1,2,4-triazole-1-yl)styryl)-5,5-dimethylcyclohex-2-enylidene)malononitrile
• CAS No.: 1428149-25-0
• Molecular Formula: C₂₁H₁₉N₅
• Molecular Weight: 341.415

Synonyms:(E)-2-(3-(4-(1H-1,2,4-triazole-1-yl)styryl)-5,5-dimethylcyclohex-2-enylidene)malononitrile

Chemical Property of (E)-2-(3-(4-(1H-1,2,4-triazole-1-yl)styryl)-5,5-dimethylcyclohex-2-enylidene)malononitrile

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Technology Process of (E)-2-(3-(4-(1H-1,2,4-triazole-1-yl)styryl)-5,5-dimethylcyclohex-2-enylidene)malononitrile

There total 2 articles about (E)-2-(3-(4-(1H-1,2,4-triazole-1-yl)styryl)-5,5-dimethylcyclohex-2-enylidene)malononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

3-dicyanomethylidene-1,5,5-trimethylcyclohexene (23051-44-7) + 4-(1H-1,2,4-triazol-1-yl)benzaldehyde (27996-86-7) → (E)-2-(3-(4-(1H-1,2,4-triazole-1-yl)styryl)-5,5-dimethylcyclohex-2-enylidene)malononitrile (1428149-25-0)

Guidance literature:

With piperidine; In acetonitrile; at 40 ℃; for 8h; Inert atmosphere;

DOI:10.1039/c3dt52364k

Reference yield:

3,5,5-Trimethylcyclohex-2-en-1-one (78-59-1) → (E)-2-(3-(4-(1H-1,2,4-triazole-1-yl)styryl)-5,5-dimethylcyclohex-2-enylidene)malononitrile (1428149-25-0)

Guidance literature:

Multi-step reaction with 2 steps

1: piperidine / ethanol / 8 h / 60 °C

2: piperidine / acetonitrile / 8 h / 40 °C / Inert atmosphere

With piperidine; In ethanol; acetonitrile;

DOI:10.1039/c3dt52364k

Reference yield: 80.0%

silver(I) hexafluorophosphate (26042-63-7) + (E)-2-(3-(4-(1H-1,2,4-triazole-1-yl)styryl)-5,5-dimethylcyclohex-2-enylidene)malononitrile (1428149-25-0) → [Ag((E)-2-(3-(4-(1H-1,2,4-triazol-1-yl)styryl)-5,5-dimethylcyclohex-2-enylidene)malononitrile)2]PF6

Guidance literature:

In dichloromethane; acetonitrile; benzene;

DOI:10.1039/c3dt52364k

upstream raw materials:

3-dicyanomethylidene-1,5,5-trimethylcyclohexene

4-(1H-1,2,4-triazol-1-yl)benzaldehyde

3,5,5-Trimethylcyclohex-2-en-1-one

Downstream raw materials:

[Ag((E)-2-(3-(4-(1H-1,2,4-triazol-1-yl)styryl)-5,5-dimethylcyclohex-2-enylidene)malononitrile)2]NO₃

[Ag((E)-2-(3-(4-(1H-1,2,4-triazol-1-yl)styryl)-5,5-dimethylcyclohex-2-enylidene)malononitrile)(CF₃CO₂)]2

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