C₃₀H₄₂O₄

Base Information

Chemical Name:C₃₀H₄₂O₄
CAS No.:1319725-93-3
Molecular Formula:C₃₀H₄₂O₄
Molecular Weight:466.661
Hs Code.:

C<sub>30</sub>H<sub>42</sub>O<sub>4</sub>

Synonyms:C₃₀H₄₂O₄

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Chemical Property of C₃₀H₄₂O₄

Chemical Property:

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Technology Process of C₃₀H₄₂O₄

There total 1 articles about C₃₀H₄₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32339-43-8
decyltriphenylphosphonium bromide

: 102207-93-2
methyl 2,3-Di-O-benzyl-β-D-ribo-pentodialdofuranoside

: 1319725-93-3
C₃₀H₄₂O₄

Guidance literature:: decyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; at 20 ℃; for 1h; Cooling with ice;

methyl 2,3-Di-O-benzyl-β-D-ribo-pentodialdofuranoside; In tetrahydrofuran; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c1ob05251a

Reference yield: 76.0%

: 1319725-93-3
C₃₀H₄₂O₄

: 1319726-00-5
C₃₀H₄₂O₅

Guidance literature:: With oxygen; palladium dichloride; In N,N-dimethyl acetamide; at 20 ℃; for 1h; under 9000.9 Torr;

C₃₀H₄₂O₄; With oxygen; In N,N-dimethyl acetamide; at 90 ℃; for 12h; under 3000.3 Torr;
DOI:10.1039/c1ob05251a

Reference yield:

: 1319725-93-3
C₃₀H₄₂O₄

: 1319726-03-8
C₃₀H₄₂O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxygen; palladium dichloride / N,N-dimethyl acetamide / 1 h / 20 °C / 9000.9 Torr

1.2: 12 h / 90 °C / 3000.3 Torr

2.1: lithium iodide / diethyl ether / 0.17 h / -40 °C / Inert atmosphere

2.2: 0.75 h / -100 °C / Inert atmosphere

2.3: -100 - 20 °C

3.1: sulfuric acid / 1,4-dioxane; water / 6 h / 20 °C / Reflux

4.1: potassium carbonate / methanol / 7 h / 20 °C / Inert atmosphere

With sulfuric acid; oxygen; potassium carbonate; palladium dichloride; lithium iodide; In 1,4-dioxane; methanol; diethyl ether; N,N-dimethyl acetamide; water;
DOI:10.1039/c1ob05251a