phenyl 4-O-acetyl-3-azido-1-thio-2,3,6-trideoxy-α-L-lyxo-hexopyranoside

Base Information

Chemical Name:phenyl 4-O-acetyl-3-azido-1-thio-2,3,6-trideoxy-α-L-lyxo-hexopyranoside
CAS No.:863503-05-3
Molecular Formula:C₁₄H₁₇N₃O₃S
Molecular Weight:307.373
Hs Code.:

Synonyms:phenyl 4-O-acetyl-3-azido-1-thio-2,3,6-trideoxy-α-L-lyxo-hexopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 4-O-acetyl-3-azido-1-thio-2,3,6-trideoxy-α-L-lyxo-hexopyranoside

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Technology Process of phenyl 4-O-acetyl-3-azido-1-thio-2,3,6-trideoxy-α-L-lyxo-hexopyranoside

There total 7 articles about phenyl 4-O-acetyl-3-azido-1-thio-2,3,6-trideoxy-α-L-lyxo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 108-98-5
thiophenol

: 179913-38-3
1,4-di-O-acetyl-3-azido-2,3,6-trideoxy-L-lyxo-hexopyranose

: 863503-05-3
phenyl 4-O-acetyl-3-azido-1-thio-2,3,6-trideoxy-α-L-lyxo-hexopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In toluene; at 20 ℃; for 2h;
DOI:10.1021/jm050144u

Reference yield:

: 127-08-2
potassium acetate

: Trifluoro-methanesulfonic acid (2S,3R,4S)-4-azido-2-methyl-6-phenylsulfanyl-tetrahydro-pyran-3-yl ester

: 863503-05-3
phenyl 4-O-acetyl-3-azido-1-thio-2,3,6-trideoxy-α-L-lyxo-hexopyranoside

: phenyl 4-O-acetyl-3-azido-1-thio-2,3,6-trideoxy-β-L-lyxo-hexopyranoside

Guidance literature:: With 18-crown-6 ether; In N,N-dimethyl-formamide; at 20 ℃; for 2h; Title compound not separated from byproducts;
DOI:10.1021/ol049187f

Reference yield:

: (4S,5S,6S)-4-Azido-6-methyl-tetrahydro-pyran-2,5-diol

: 863503-05-3
phenyl 4-O-acetyl-3-azido-1-thio-2,3,6-trideoxy-α-L-lyxo-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 2.05 g / pyridine; DMAP

2: 80 percent / BF₃*Et₂O / toluene / 0 - 20 °C

With pyridine; dmap; boron trifluoride diethyl etherate; In toluene;
DOI:10.1016/j.bmc.2005.08.014