N-(m-tolyl)-2-(4-{[N-(2,2,4-trimethyl-7-phenoxy-1,2-dihydroquinolin-6-yl)methanesulfonamido]methyl}-1H-1,2,3-triazol-1-yl)acetamide

Base Information

Chemical Name:N-(m-tolyl)-2-(4-{[N-(2,2,4-trimethyl-7-phenoxy-1,2-dihydroquinolin-6-yl)methanesulfonamido]methyl}-1H-1,2,3-triazol-1-yl)acetamide
CAS No.:1601552-71-9
Molecular Formula:C₃₁H₃₄N₆O₄S
Molecular Weight:586.715
Hs Code.:

Synonyms:N-(m-tolyl)-2-(4-{[N-(2,2,4-trimethyl-7-phenoxy-1,2-dihydroquinolin-6-yl)methanesulfonamido]methyl}-1H-1,2,3-triazol-1-yl)acetamide

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Chemical Property of N-(m-tolyl)-2-(4-{[N-(2,2,4-trimethyl-7-phenoxy-1,2-dihydroquinolin-6-yl)methanesulfonamido]methyl}-1H-1,2,3-triazol-1-yl)acetamide

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Technology Process of N-(m-tolyl)-2-(4-{[N-(2,2,4-trimethyl-7-phenoxy-1,2-dihydroquinolin-6-yl)methanesulfonamido]methyl}-1H-1,2,3-triazol-1-yl)acetamide

There total 4 articles about N-(m-tolyl)-2-(4-{[N-(2,2,4-trimethyl-7-phenoxy-1,2-dihydroquinolin-6-yl)methanesulfonamido]methyl}-1H-1,2,3-triazol-1-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1601552-75-3
C₂₂H₂₄N₂O₃S

: 1211462-24-6
C₉H₁₀N₄O

: 1601552-71-9
N-(m-tolyl)-2-(4-{[N-(2,2,4-trimethyl-7-phenoxy-1,2-dihydroquinolin-6-yl)methanesulfonamido]methyl}-1H-1,2,3-triazol-1-yl)acetamide

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.bioorg.2013.12.002

Reference yield:

: 51803-78-2
nimesulide

: 1601552-71-9
N-(m-tolyl)-2-(4-{[N-(2,2,4-trimethyl-7-phenoxy-1,2-dihydroquinolin-6-yl)methanesulfonamido]methyl}-1H-1,2,3-triazol-1-yl)acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone / 20 °C

2: tin; hydrogenchloride / 6 h / 90 °C

3: ammonium cerium (IV) nitrate / 20 h / 50 - 55 °C

4: copper(ll) sulfate pentahydrate; sodium L-ascorbate / N,N-dimethyl-formamide; water / 20 °C

With hydrogenchloride; tin; copper(ll) sulfate pentahydrate; ammonium cerium (IV) nitrate; potassium carbonate; sodium L-ascorbate; In water; N,N-dimethyl-formamide; acetone; 3: |Skraup Quinoline Synthesis;
DOI:10.1016/j.bioorg.2013.12.002

Reference yield:

: 1601552-74-2
C₁₆H₁₄N₂O₅S

: 1601552-71-9
N-(m-tolyl)-2-(4-{[N-(2,2,4-trimethyl-7-phenoxy-1,2-dihydroquinolin-6-yl)methanesulfonamido]methyl}-1H-1,2,3-triazol-1-yl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: tin; hydrogenchloride / 6 h / 90 °C

2: ammonium cerium (IV) nitrate / 20 h / 50 - 55 °C

3: copper(ll) sulfate pentahydrate; sodium L-ascorbate / N,N-dimethyl-formamide; water / 20 °C

With hydrogenchloride; tin; copper(ll) sulfate pentahydrate; ammonium cerium (IV) nitrate; sodium L-ascorbate; In water; N,N-dimethyl-formamide; 2: |Skraup Quinoline Synthesis;
DOI:10.1016/j.bioorg.2013.12.002