{(Z)-1,3-Diphenyl-3-[(Z)-trimethylsilanyl-imino]-propenyl}-trimethylsilanyl-amine

Base Information

• Chemical Name: {(Z)-1,3-Diphenyl-3-[(Z)-trimethylsilanyl-imino]-propenyl}-trimethylsilanyl-amine
• CAS No.: 226717-80-2
• Molecular Formula: C₂₁H₃₀N₂Si₂
• Molecular Weight: 366.654
• Mol file: 226717-80-2.mol

Synonyms:{(Z)-1,3-Diphenyl-3-[(Z)-trimethylsilanyl-imino]-propenyl}-trimethylsilanyl-amine

Chemical Property of {(Z)-1,3-Diphenyl-3-[(Z)-trimethylsilanyl-imino]-propenyl}-trimethylsilanyl-amine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of {(Z)-1,3-Diphenyl-3-[(Z)-trimethylsilanyl-imino]-propenyl}-trimethylsilanyl-amine

There total 3 articles about {(Z)-1,3-Diphenyl-3-[(Z)-trimethylsilanyl-imino]-propenyl}-trimethylsilanyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

C21H29N2Si2(1-)*K(1+) → {(Z)-1,3-Diphenyl-3-[(Z)-trimethylsilanyl-imino]-propenyl}-trimethylsilanyl-amine (226717-80-2)

Guidance literature:

With ethylene dibromide; In hexane; at 50 ℃; for 5h;

DOI:10.1016/j.jorganchem.2004.05.042

Reference yield: 95.0%

[(N(SiMe3)C(Ph))2CH]Li → {(Z)-1,3-Diphenyl-3-[(Z)-trimethylsilanyl-imino]-propenyl}-trimethylsilanyl-amine (226717-80-2)

Guidance literature:

With cyclopenta-1,3-diene; In pentane; at 20 ℃; for 12h;

DOI:10.1039/b601881e

Reference yield:

benzonitrile (100-47-0) + [K{CH(SiMe3)2}] (118111-55-0) → {(Z)-1,3-Diphenyl-3-[(Z)-trimethylsilanyl-imino]-propenyl}-trimethylsilanyl-amine (226717-80-2)

Guidance literature:

With (CH₂Br₂)2; Yield given. Multistep reaction; 1.) ether, 0 deg C, 2 h, 2.) hexane, 50 deg C, 5 h;

DOI:10.1039/c39940001699

upstream raw materials:

benzonitrile

[K{CH(SiMe₃)2}]