N-[3-(2,5-Dihydroxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide

Base Information

Chemical Name:N-[3-(2,5-Dihydroxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide
CAS No.:121746-67-6
Molecular Formula:C₁₉H₂₃NO₃
Molecular Weight:313.397
Hs Code.:

Synonyms:N-[3-(2,5-Dihydroxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide

Suppliers and Price of N-[3-(2,5-Dihydroxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-[3-(2,5-Dihydroxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-[3-(2,5-Dihydroxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide

There total 6 articles about N-[3-(2,5-Dihydroxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 121746-60-9
N-[3-(2,5-Bis-benzyloxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide

: 121746-67-6
N-[3-(2,5-Dihydroxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; under 760 Torr; Ambient temperature;
DOI:10.1002/ardp.19893220405

Reference yield:

: 40930-93-6
2,5-bis(benzyloxy)-4-methyl-benzaldehyde

: 121746-67-6
N-[3-(2,5-Dihydroxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / 30percent aq. NaOH / 3 h / Ambient temperature

2: 85 percent / H₂ / PtO₂ / tetrahydrofuran

3: 1.) p-TosOH, 2.) LiAlH₄ / 1.) toluene, reflux, 2.) ether, r.t., 48 h

4: 55 percent / 3 h / Heating

5: 64 percent / H₂ / 10percent Pd/C / tetrahydrofuran / 760 Torr / Ambient temperature

With sodium hydroxide; lithium aluminium tetrahydride; hydrogen; toluene-4-sulfonic acid; platinum(IV) oxide; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1002/ardp.19893220405

Reference yield:

: 62-53-3
aniline

: 121746-67-6
N-[3-(2,5-Dihydroxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) p-TosOH, 2.) LiAlH₄ / 1.) toluene, reflux, 2.) ether, r.t., 48 h

2: 55 percent / 3 h / Heating

3: 64 percent / H₂ / 10percent Pd/C / tetrahydrofuran / 760 Torr / Ambient temperature

With lithium aluminium tetrahydride; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1002/ardp.19893220405