N-[3-(2,5-Bis-benzyloxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide

Base Information

Chemical Name:N-[3-(2,5-Bis-benzyloxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide
CAS No.:121746-60-9
Molecular Formula:C₃₃H₃₅NO₃
Molecular Weight:493.646
Hs Code.:

Synonyms:N-[3-(2,5-Bis-benzyloxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide

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Chemical Property of N-[3-(2,5-Bis-benzyloxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide

Chemical Property:

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Technology Process of N-[3-(2,5-Bis-benzyloxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide

There total 4 articles about N-[3-(2,5-Bis-benzyloxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 108-24-7
acetic anhydride

: 121746-56-3
[3-(2,5-Bis-benzyloxy-4-methyl-phenyl)-1-methyl-propyl]-phenyl-amine

: 121746-60-9
N-[3-(2,5-Bis-benzyloxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide

Guidance literature:: for 3h; Heating;
DOI:10.1002/ardp.19893220405

Reference yield:

: 40930-93-6
2,5-bis(benzyloxy)-4-methyl-benzaldehyde

: 121746-60-9
N-[3-(2,5-Bis-benzyloxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / 30percent aq. NaOH / 3 h / Ambient temperature

2: 85 percent / H₂ / PtO₂ / tetrahydrofuran

3: 1.) p-TosOH, 2.) LiAlH₄ / 1.) toluene, reflux, 2.) ether, r.t., 48 h

4: 55 percent / 3 h / Heating

With sodium hydroxide; lithium aluminium tetrahydride; hydrogen; toluene-4-sulfonic acid; platinum(IV) oxide; In tetrahydrofuran;
DOI:10.1002/ardp.19893220405

Reference yield:

: 62-53-3
aniline

: 121746-60-9
N-[3-(2,5-Bis-benzyloxy-4-methyl-phenyl)-1-methyl-propyl]-N-phenyl-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) p-TosOH, 2.) LiAlH₄ / 1.) toluene, reflux, 2.) ether, r.t., 48 h

2: 55 percent / 3 h / Heating

With lithium aluminium tetrahydride; toluene-4-sulfonic acid;
DOI:10.1002/ardp.19893220405