O₂-(2,4-dinitrophenyl) 1-[N-(2-hydroxyethyl)-N-methylamino]diazen-1-ium-1,2-diolate

Base Information

• Chemical Name: O₂-(2,4-dinitrophenyl) 1-[N-(2-hydroxyethyl)-N-methylamino]diazen-1-ium-1,2-diolate
• CAS No.: 1083159-15-2
• Molecular Formula: C₉H₁₁N₅O₇
• Molecular Weight: 301.216

Synonyms:O₂-(2,4-dinitrophenyl) 1-[N-(2-hydroxyethyl)-N-methylamino]diazen-1-ium-1,2-diolate

Chemical Property of O₂-(2,4-dinitrophenyl) 1-[N-(2-hydroxyethyl)-N-methylamino]diazen-1-ium-1,2-diolate

Chemical Property:

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Technology Process of O₂-(2,4-dinitrophenyl) 1-[N-(2-hydroxyethyl)-N-methylamino]diazen-1-ium-1,2-diolate

There total 1 articles about O₂-(2,4-dinitrophenyl) 1-[N-(2-hydroxyethyl)-N-methylamino]diazen-1-ium-1,2-diolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

1-hydroxy-[3-(2-hydroxyethyl)-3-methyl]-1-triazene 2-oxide sodium salt (742081-66-9) + 2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) → O2-(2,4-dinitrophenyl) 1-[N-(2-hydroxyethyl)-N-methylamino]diazen-1-ium-1,2-diolate (1083159-15-2)

Guidance literature:

With sodium hydrogencarbonate; In water; tert-butyl alcohol; Cooling with ice;

DOI:10.1021/ol8020989

Reference yield: 68.0%

O2-(2,4-dinitrophenyl) 1-[N-(2-hydroxyethyl)-N-methylamino]diazen-1-ium-1,2-diolate (1083159-15-2) → O2-(2,4-dinitrophenyl) 1-[N-(carboxymethyl)-N-methylamino]diazen-1-ium-1,2-diolate (1083159-08-3)

Guidance literature:

With sodium periodate; ruthenium(III) chloride monohydrate; In water; ethyl acetate; acetonitrile;

DOI:10.1021/ol8020989

upstream raw materials:

1-hydroxy-[3-(2-hydroxyethyl)-3-methyl]-1-triazene 2-oxide sodium salt

2,4-Dinitrofluorobenzene

Downstream raw materials:

O₂-(2,4-dinitrophenyl) 1-[N-(carboxymethyl)-N-methylamino]diazen-1-ium-1,2-diolate

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