N-[2-amino-6-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(4-methoxy-phenyl)-acetamide

Base Information

• Chemical Name: N-[2-amino-6-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(4-methoxy-phenyl)-acetamide
• CAS No.: 840523-21-9
• Molecular Formula: C₂₁H₃₀N₂O₃Si
• Molecular Weight: 386.566

Synonyms:N-[2-amino-6-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(4-methoxy-phenyl)-acetamide

Chemical Property of N-[2-amino-6-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(4-methoxy-phenyl)-acetamide

Chemical Property:

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Technology Process of N-[2-amino-6-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(4-methoxy-phenyl)-acetamide

There total 3 articles about N-[2-amino-6-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(4-methoxy-phenyl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[2-(tert-butyl-dimethyl-silanyloxy)-6-nitro-phenyl]-2-(4-methoxy-phenyl)-acetamide (840523-20-8) → N-[2-amino-6-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(4-methoxy-phenyl)-acetamide (840523-21-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; under 775.722 Torr;

DOI:10.1016/j.bmcl.2005.08.067

Reference yield:

N-(2-hydroxy-6-nitro-phenyl)-2-(4-methoxy-phenyl)-acetamide (840523-19-5) → N-[2-amino-6-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(4-methoxy-phenyl)-acetamide (840523-21-9)

Guidance literature:

Multi-step reaction with 2 steps

1: imidazole

2: H₂ / Pd/C / ethanol / 775.72 Torr

With 1H-imidazole; hydrogen; palladium on activated charcoal; In ethanol;

DOI:10.1016/j.bmcl.2005.08.067

Reference yield:

2-Amino-3-nitrophenol (603-85-0) → N-[2-amino-6-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(4-methoxy-phenyl)-acetamide (840523-21-9)

Guidance literature:

Multi-step reaction with 3 steps

1: imidazole

2: H₂ / Pd/C / ethanol / 775.72 Torr

With 1H-imidazole; hydrogen; palladium on activated charcoal; In ethanol;

DOI:10.1016/j.bmcl.2005.08.067

upstream raw materials:

N-[2-(tert-butyl-dimethyl-silanyloxy)-6-nitro-phenyl]-2-(4-methoxy-phenyl)-acetamide

N-(2-hydroxy-6-nitro-phenyl)-2-(4-methoxy-phenyl)-acetamide

2-Amino-3-nitrophenol

Downstream raw materials:

3-amino-2-[2-(4-methoxy-phenyl)-ethylamino]-phenol

3-(tert-butyl-dimethyl-silanyloxy)-N²-[2-(4-methoxy-phenyl)-ethyl]-benzene-1,2-diamine

3-[2-(4-methoxy-phenyl)-ethyl]-3H-benzotriazol-4-ol

7-(tert-butyl-dimethyl-silanyloxy)-1-[2-(4-methoxy-phenyl)-ethyl]-1,3-dihydro-benzoimidazol-2-one

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