Technology Process of C17H23F5NO6P
There total 4 articles about C17H23F5NO6P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
acetonitrile;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: toluene-4-sulfonic acid / toluene / 2 h / Inert atmosphere; Reflux
1.2: pH 9
2.1: 1-butyl-3-methylimidazolium Tetrafluoroborate / 3 h / 150 °C
3.1: hydrogen / platinum on carbon / methanol / 16 h / 20 °C
4.1: hydrogenchloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 1 h / 20 °C
With
hydrogenchloride; hydrogen; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-butyl-3-methylimidazolium Tetrafluoroborate;
platinum on carbon;
In
methanol; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogen / platinum on carbon / methanol / 16 h / 20 °C
2: hydrogenchloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 1 h / 20 °C
With
hydrogenchloride; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
platinum on carbon;
In
methanol; acetonitrile;