C₂₁H₃₅N₃O₃

Base Information

Chemical Name:C₂₁H₃₅N₃O₃
CAS No.:1271773-36-4
Molecular Formula:C₂₁H₃₅N₃O₃
Molecular Weight:377.527
Hs Code.:

C<sub>21</sub>H<sub>35</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:C₂₁H₃₅N₃O₃

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Chemical Property of C₂₁H₃₅N₃O₃

Chemical Property:

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Technology Process of C₂₁H₃₅N₃O₃

There total 9 articles about C₂₁H₃₅N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7328-91-8
2,2-Dimethyl-1,3-diaminopropane

: 1271773-33-1
3-{[(tert-butoxycarbonyl)amino]methyl}-4-phenylbutanoic acid

: 1271773-36-4
C₂₁H₃₅N₃O₃

Guidance literature:: 3-{[(tert-butoxycarbonyl)amino]methyl}-4-phenylbutanoic acid; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 1h;

2,2-Dimethyl-1,3-diaminopropane; In dichloromethane; at 0 - 20 ℃; for 18h;

Reference yield:

: 1271773-08-0
C₂₁H₂₁NO₃

: 1271773-36-4
C₂₁H₃₅N₃O₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / -78 - 20 °C

2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 16 h / 0 - 20 °C

3.1: hydrazine hydrate / ethanol / 3 h / Heating; Reflux

4.1: sodium hydrogencarbonate / 1,4-dioxane; water / 5 h

5.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; tert-butyl alcohol; tetrahydrofuran / 16 h / 0 - 20 °C

6.1: sodium periodate / water; tetrahydrofuran / 3.5 h / 0 °C

7.1: pyridinium chlorochromate / dichloromethane / 20 °C / Molecular sieves 3?

8.1: water; lithium hydroxide / tetrahydrofuran / 2 h / 20 °C

9.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 1 h / 0 °C

9.2: 18 h / 0 - 20 °C

With sodium periodate; osmium(VIII) oxide; lithium aluminium tetrahydride; water; sodium hydrogencarbonate; benzotriazol-1-ol; hydrazine hydrate; 4-methylmorpholine N-oxide; dicyclohexyl-carbodiimide; triphenylphosphine; pyridinium chlorochromate; lithium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; tert-butyl alcohol;

Reference yield:

: (S)-2-allyl-3-phenylpropan-1-ol

: 1271773-36-4
C₂₁H₃₅N₃O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 16 h / 0 - 20 °C

2.1: hydrazine hydrate / ethanol / 3 h / Heating; Reflux

3.1: sodium hydrogencarbonate / 1,4-dioxane; water / 5 h

4.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; tert-butyl alcohol; tetrahydrofuran / 16 h / 0 - 20 °C

5.1: sodium periodate / water; tetrahydrofuran / 3.5 h / 0 °C

6.1: pyridinium chlorochromate / dichloromethane / 20 °C / Molecular sieves 3?

7.1: water; lithium hydroxide / tetrahydrofuran / 2 h / 20 °C

8.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 1 h / 0 °C

8.2: 18 h / 0 - 20 °C

With sodium periodate; osmium(VIII) oxide; water; sodium hydrogencarbonate; benzotriazol-1-ol; hydrazine hydrate; 4-methylmorpholine N-oxide; dicyclohexyl-carbodiimide; triphenylphosphine; pyridinium chlorochromate; lithium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; tert-butyl alcohol;