3-(p-dimethylaminophenylethenyl)pyrido<3,2,1-j,k>carbazolium chloride

Base Information

• Chemical Name: 3-(p-dimethylaminophenylethenyl)pyrido<3,2,1-j,k>carbazolium chloride
• CAS No.: 113544-78-8
• Molecular Formula: C₂₅H₂₁N₂*Cl
• Molecular Weight: 384.908
• Mol file: 113544-78-8.mol

Synonyms:3-(p-dimethylaminophenylethenyl)pyrido<3,2,1-j,k>carbazolium chloride

Chemical Property of 3-(p-dimethylaminophenylethenyl)pyrido<3,2,1-j,k>carbazolium chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(p-dimethylaminophenylethenyl)pyrido<3,2,1-j,k>carbazolium chloride

There total 2 articles about 3-(p-dimethylaminophenylethenyl)pyrido<3,2,1-j,k>carbazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

3-methylpyrido<3,2,1-j,k>carbazolium chloride (82899-43-2) + 4-dimethylamino-benzaldehyde (100-10-7) → 3-(p-dimethylaminophenylethenyl)pyrido<3,2,1-j,k>carbazolium chloride (113544-78-8)

Guidance literature:

With acetic anhydride; at 100 ℃; for 0.5h;

DOI:10.1007/BF00769653

Reference yield:

9H-carbazole (86-74-8,105184-46-1,97960-57-1) → 3-(p-dimethylaminophenylethenyl)pyrido<3,2,1-j,k>carbazolium chloride (113544-78-8)

Guidance literature:

Multi-step reaction with 2 steps

1: concentrated hydrochloric acid, nitrobenzene / butan-1-ol / 7 h / 100 °C

2: 69 percent / acetic anhydride / 0.5 h / Heating

With hydrogenchloride; nitrobenzene; In acetic anhydride; butan-1-ol;

DOI:10.1007/BF00473454

upstream raw materials:

3-methylpyrido<3,2,1-j,k>carbazolium chloride

4-dimethylamino-benzaldehyde

9H-carbazole