N,N,N',N'-tetraethyl-2,4,10,12-tetraoxa-3,11-diphospha-tricyclo[11.3.1.1^5,9]octadeca-1⁽¹⁷⁾,5,7,9⁽¹⁸⁾,13,15-hexaene-3,11-diamine

Base Information

• Chemical Name: N,N,N',N'-tetraethyl-2,4,10,12-tetraoxa-3,11-diphospha-tricyclo[11.3.1.1^5,9]octadeca-1⁽¹⁷⁾,5,7,9⁽¹⁸⁾,13,15-hexaene-3,11-diamine
• CAS No.: 244217-61-6
• Molecular Formula: C₂₀H₂₈N₂O₄P₂
• Molecular Weight: 422.401

Synonyms:N,N,N',N'-tetraethyl-2,4,10,12-tetraoxa-3,11-diphospha-tricyclo[11.3.1.1^5,9]octadeca-1⁽¹⁷⁾,5,7,9⁽¹⁸⁾,13,15-hexaene-3,11-diamine

Chemical Property of N,N,N',N'-tetraethyl-2,4,10,12-tetraoxa-3,11-diphospha-tricyclo[11.3.1.1^5,9]octadeca-1⁽¹⁷⁾,5,7,9⁽¹⁸⁾,13,15-hexaene-3,11-diamine

Chemical Property:

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Technology Process of N,N,N',N'-tetraethyl-2,4,10,12-tetraoxa-3,11-diphospha-tricyclo[11.3.1.1^5,9]octadeca-1⁽¹⁷⁾,5,7,9⁽¹⁸⁾,13,15-hexaene-3,11-diamine

There total 2 articles about N,N,N',N'-tetraethyl-2,4,10,12-tetraoxa-3,11-diphospha-tricyclo[11.3.1.1^5,9]octadeca-1⁽¹⁷⁾,5,7,9⁽¹⁸⁾,13,15-hexaene-3,11-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

resorcinol bis(tetraethylphosphodiamidite) (194033-62-0) → hexaethylphosphoric triamide (2283-11-6) + N,N,N',N'-tetraethyl-2,4,10,12-tetraoxa-3,11-diphospha-tricyclo[11.3.1.15,9]octadeca-1(17),5,7,9(18),13,15-hexaene-3,11-diamine (244217-61-6)

Guidance literature:

In acetonitrile; at 20 ℃; for 600h; Title compound not separated from byproducts.;

DOI:10.1134/S1070363206020046

Reference yield:

p-xylylene glycol (589-29-7) + hexaethylphosphoric triamide (2283-11-6) + recorcinol (108-46-3) → C30H42O6N2P2 + N,N,N',N'-tetraethyl-2,4,10,12-tetraoxa-3,11-diphospha-tricyclo[11.3.1.15,9]octadeca-1(17),5,7,9(18),13,15-hexaene-3,11-diamine (244217-61-6)

Guidance literature:

hexaethylphosphoric triamide; recorcinol; In acetonitrile; at 20 ℃; for 1h;

p-xylylene glycol; In acetonitrile; at 20 ℃; for 120h; Further stages.;

DOI:10.1134/S1070363207060126

upstream raw materials:

resorcinol bis(tetraethylphosphodiamidite)

p-xylylene glycol

hexaethylphosphoric triamide

recorcinol

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