3,5-didodecyl-2,6-diformylphenol

Base Information

Chemical Name:3,5-didodecyl-2,6-diformylphenol
CAS No.:1310421-09-0
Molecular Formula:C₃₂H₅₄O₃
Molecular Weight:486.779
Hs Code.:

Synonyms:3,5-didodecyl-2,6-diformylphenol

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Chemical Property of 3,5-didodecyl-2,6-diformylphenol

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Technology Process of 3,5-didodecyl-2,6-diformylphenol

There total 4 articles about 3,5-didodecyl-2,6-diformylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 100-97-0
hexamethylenetetramine

: 52066-77-0
3,5-didodecylphenol

: 1310421-09-0
3,5-didodecyl-2,6-diformylphenol

Guidance literature:: hexamethylenetetramine; 3,5-didodecylphenol; With trifluoroacetic acid; at 100 ℃; for 24h; Inert atmosphere;

With hydrogenchloride; water; In trifluoroacetic acid; at 100 ℃; for 24h;
DOI:10.1002/anie.201100827

Reference yield:

: 1150657-98-9
3,5-dibromo-(tetrahydro-2H-pyran-2-yloxy)benzene

: 1310421-09-0
3,5-didodecyl-2,6-diformylphenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran / 72 h / 75 °C / Inert atmosphere

2.1: methanol; toluene-4-sulfonic acid / tetrahydrofuran / 1 h / 25 °C

3.1: trifluoroacetic acid / 24 h / 100 °C / Inert atmosphere

3.2: 24 h / 100 °C

With methanol; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; toluene-4-sulfonic acid; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1002/anie.201100827

Reference yield:

: 626-41-5
3,5-dibromophenol

: 1310421-09-0
3,5-didodecyl-2,6-diformylphenol

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / dichloromethane / 3.5 h / 0 - 25 °C

2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran / 72 h / 75 °C / Inert atmosphere

3.1: methanol; toluene-4-sulfonic acid / tetrahydrofuran / 1 h / 25 °C

4.1: trifluoroacetic acid / 24 h / 100 °C / Inert atmosphere

4.2: 24 h / 100 °C

With methanol; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; toluene-4-sulfonic acid; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201100827