N-(2-chlorophenyl)-2-nitrobenzamide

Base Information

Chemical Name:N-(2-chlorophenyl)-2-nitrobenzamide
CAS No.:50622-99-6
Molecular Formula:C₁₃H₉ClN₂O₃
Molecular Weight:276.679
Hs Code.:
DSSTox Substance ID:DTXSID001035098
Nikkaji Number:J1.570.996K

Synonyms:N-(2-chlorophenyl)-2-nitrobenzamide;50622-99-6;Benzamide, N-(2-chlorophenyl)-2-nitro-;CBMicro_009344;Cambridge id 5137218;Oprea1_199536;Oprea1_359938;2'-Chloro-2-nitrobenzanilide;DTXSID001035098;SMSF0003655;MFCD00432335;AKOS002516630;CB12459;LS-07281;BIM-0009523.P001;CS-0323033;SR-01000196617;SR-01000196617-1

Suppliers and Price of N-(2-chlorophenyl)-2-nitrobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of N-(2-chlorophenyl)-2-nitrobenzamide

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:276.0301698
Heavy Atom Count:19
Complexity:345

Purity/Quality:: 98%+ ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(=O)NC2=CC=CC=C2Cl)[N+](=O)[O-]

Technology Process of N-(2-chlorophenyl)-2-nitrobenzamide

There total 3 articles about N-(2-chlorophenyl)-2-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95-51-2
o-chloroaniline

: 610-14-0
2-nitrobenzyl chloride

: 50622-99-6
2-nitro-benzoic acid-(2-chloro-anilide)

Guidance literature:: DOI:10.1039/jr9520004059

Reference yield:

: 552-16-9,104810-18-6
ortho-nitrobenzoic acid

: 50622-99-6
2-nitro-benzoic acid-(2-chloro-anilide)

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 0 - 20 °C

2: triethylamine / dichloromethane

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1039/c6ra00855k