C₄₂H₇₉NO₃Si₃

Base Information

Chemical Name:C₄₂H₇₉NO₃Si₃
CAS No.:1448446-18-1
Molecular Formula:C₄₂H₇₉NO₃Si₃
Molecular Weight:730.351
Hs Code.:

C<sub>42</sub>H<sub>79</sub>NO<sub>3</sub>Si<sub>3</sub>

Synonyms:C₄₂H₇₉NO₃Si₃

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Chemical Property of C₄₂H₇₉NO₃Si₃

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Technology Process of C₄₂H₇₉NO₃Si₃

There total 12 articles about C₄₂H₇₉NO₃Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1448446-17-0
C₄₁H₇₆BrNO₃Si₃

: 544-97-8
dimethyl zinc(II)

: 1448446-18-1
C₄₂H₇₉NO₃Si₃

Guidance literature:: With bis(tri-t-butylphosphine)palladium⁽⁰⁾; In tetrahydrofuran; toluene; at 0 ℃; for 4.5h; stereoselective reaction; Inert atmosphere;

Reference yield:

: 138124-05-7
(1S,6R)-(-)-8-Oxabicyclo<4.3.0>non-2-en-7-one

: 1448446-18-1
C₄₂H₇₉NO₃Si₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - -30 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane / 0.42 h / -78 °C / Inert atmosphere

3.1: diisopropylamine / diethyl ether; tetrahydrofuran; hexane / 0.33 h / -78 - -50 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

4.2: -78 - 20 °C / Inert atmosphere

5.1: hydrogenchloride / tetrahydrofuran; water / 0.25 h / 20 °C

6.1: dimethyl sulfoxide; oxalyl dichloride; N-ethyl-N,N-diisopropylamine / dichloromethane / -78 - 20 °C / Inert atmosphere

7.1: triphenylphosphine; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

8.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; thallium (I) ethoxide / tetrahydrofuran; water / 20 °C / Inert atmosphere

9.1: bis(tri-t-butylphosphine)palladium⁽⁰⁾ / toluene; tetrahydrofuran / 4.5 h / 0 °C / Inert atmosphere

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; oxalyl dichloride; bis(tri-t-butylphosphine)palladium⁽⁰⁾; thallium (I) ethoxide; diisobutylaluminium hydride; dimethyl sulfoxide; diisopropylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; toluene; 8.1: |Suzuki Coupling / 9.1: |Negishi Coupling;

Reference yield:

: 1448446-08-9
C₃₀H₆₂BNO₅Si₂

: 1448446-18-1
C₄₂H₇₉NO₃Si₃

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; thallium (I) ethoxide / tetrahydrofuran; water / 20 °C / Inert atmosphere

2: bis(tri-t-butylphosphine)palladium⁽⁰⁾ / toluene; tetrahydrofuran / 4.5 h / 0 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis(tri-t-butylphosphine)palladium⁽⁰⁾; thallium (I) ethoxide; In tetrahydrofuran; water; toluene; 1: |Suzuki Coupling / 2: |Negishi Coupling;