N-[4-(aminosulfonyl)-2-methylphenyl]-2-[(6-bromo-1-(3,5-dimethylbenzoyl)-2-naphthalenyl)oxy]acetamide

Base Information

• Chemical Name: N-[4-(aminosulfonyl)-2-methylphenyl]-2-[(6-bromo-1-(3,5-dimethylbenzoyl)-2-naphthalenyl)oxy]acetamide
• CAS No.: 1322667-67-3
• Molecular Formula: C₂₈H₂₅BrN₂O₅S
• Molecular Weight: 581.487

Synonyms:N-[4-(aminosulfonyl)-2-methylphenyl]-2-[(6-bromo-1-(3,5-dimethylbenzoyl)-2-naphthalenyl)oxy]acetamide

Chemical Property of N-[4-(aminosulfonyl)-2-methylphenyl]-2-[(6-bromo-1-(3,5-dimethylbenzoyl)-2-naphthalenyl)oxy]acetamide

Chemical Property:

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Technology Process of N-[4-(aminosulfonyl)-2-methylphenyl]-2-[(6-bromo-1-(3,5-dimethylbenzoyl)-2-naphthalenyl)oxy]acetamide

There total 3 articles about N-[4-(aminosulfonyl)-2-methylphenyl]-2-[(6-bromo-1-(3,5-dimethylbenzoyl)-2-naphthalenyl)oxy]acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.9%

N-[4-(aminosulfonyl)-2-methylphenyl]-2-bromoacetamide (329944-57-2) + C19H15BrO2 (1322667-86-6) → N-[4-(aminosulfonyl)-2-methylphenyl]-2-[(6-bromo-1-(3,5-dimethylbenzoyl)-2-naphthalenyl)oxy]acetamide (1322667-67-3)

Guidance literature:

With potassium carbonate; sodium iodide; In acetone; for 2h; Reflux;

DOI:10.1016/j.bmc.2011.06.007

Reference yield:

2-Bromo-6-methoxynaphthalene (5111-65-9) → N-[4-(aminosulfonyl)-2-methylphenyl]-2-[(6-bromo-1-(3,5-dimethylbenzoyl)-2-naphthalenyl)oxy]acetamide (1322667-67-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: aluminum (III) chloride / carbon disulfide / 2 h / 5 °C / Reflux

1.2: 0.5 h / Cooling with ice

2.1: potassium carbonate; sodium iodide / acetone / 2 h / Reflux

With aluminum (III) chloride; potassium carbonate; sodium iodide; In carbon disulfide; acetone; 1.1: Friedel-Crafts acylation;

DOI:10.1016/j.bmc.2011.06.007

Reference yield:

3,5-dimethylbenzoyl chloride (6613-44-1) → N-[4-(aminosulfonyl)-2-methylphenyl]-2-[(6-bromo-1-(3,5-dimethylbenzoyl)-2-naphthalenyl)oxy]acetamide (1322667-67-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: aluminum (III) chloride / carbon disulfide / 2 h / 5 °C / Reflux

1.2: 0.5 h / Cooling with ice

2.1: potassium carbonate; sodium iodide / acetone / 2 h / Reflux

With aluminum (III) chloride; potassium carbonate; sodium iodide; In carbon disulfide; acetone; 1.1: Friedel-Crafts acylation;

DOI:10.1016/j.bmc.2011.06.007

upstream raw materials:

N-[4-(aminosulfonyl)-2-methylphenyl]-2-bromoacetamide

C₁₉H₁₅BrO₂

2-Bromo-6-methoxynaphthalene

3,5-dimethylbenzoyl chloride

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