Technology Process of 4-formyl-3-isopropoxy-N,N-diisopropylbenzamide
There total 8 articles about 4-formyl-3-isopropoxy-N,N-diisopropylbenzamide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium periodate; osmium(VIII) oxide;
In
tetrachloromethane; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2003.09.096
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: 90 percent / Cs2CO3 / acetone / 10 h / Heating
2.1: aq. H2SO4; NaNO2 / methanol / 0.25 h / 0 °C
2.2: 86 percent / KI; Cu / methanol / 8 h / Heating
3.1: 95 percent / Pd(PPh3)4 / toluene / 12 h / Heating
4.1: aq. NaOH / methanol / 20 °C
5.1: oxalyl chloride; DMF / CH2Cl2 / 2 h / 20 °C
6.1: 2.04 g / CH2Cl2 / 3 h / 20 °C
7.1: OsO4 / 2-methyl-propan-2-ol; CCl4; H2O / 0.25 h / 20 °C
8.1: NaIO4 / 2-methyl-propan-2-ol; CCl4; H2O
With
sodium hydroxide; sodium periodate; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium(0); oxalyl dichloride; sulfuric acid; caesium carbonate; N,N-dimethyl-formamide; sodium nitrite;
In
methanol; tetrachloromethane; dichloromethane; water; acetone; toluene; tert-butyl alcohol;
2.2: Sandmeyer reaction / 3.1: Stille coupling;
DOI:10.1021/ja0446404
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 2.04 g / CH2Cl2 / 3 h / 20 °C
2: OsO4 / 2-methyl-propan-2-ol; CCl4; H2O / 0.25 h / 20 °C
3: NaIO4 / 2-methyl-propan-2-ol; CCl4; H2O
With
sodium periodate; osmium(VIII) oxide;
In
tetrachloromethane; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ja0446404
