2-amino-3-({4-[2-(4-tert-butylphenyl)-1H-benzimidazol-4-yl]piperazin-1-yl}methyl)phenylamine

Base Information

• Chemical Name: 2-amino-3-({4-[2-(4-tert-butylphenyl)-1H-benzimidazol-4-yl]piperazin-1-yl}methyl)phenylamine
• CAS No.: 874279-71-7
• Molecular Formula: C₂₈H₃₄N₆
• Molecular Weight: 454.618

Synonyms:2-amino-3-({4-[2-(4-tert-butylphenyl)-1H-benzimidazol-4-yl]piperazin-1-yl}methyl)phenylamine

Chemical Property of 2-amino-3-({4-[2-(4-tert-butylphenyl)-1H-benzimidazol-4-yl]piperazin-1-yl}methyl)phenylamine

Chemical Property:

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Technology Process of 2-amino-3-({4-[2-(4-tert-butylphenyl)-1H-benzimidazol-4-yl]piperazin-1-yl}methyl)phenylamine

There total 1 articles about 2-amino-3-({4-[2-(4-tert-butylphenyl)-1H-benzimidazol-4-yl]piperazin-1-yl}methyl)phenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

2-({4-[2-(4-tert-butylphenyl)-1H-benzo[d]imidazol-4-yl]piperazin-1-yl}methyl)-6-nitrophenylamine (874279-70-6) → 2-amino-3-({4-[2-(4-tert-butylphenyl)-1H-benzimidazol-4-yl]piperazin-1-yl}methyl)phenylamine (874279-71-7)

Guidance literature:

With tin(ll) chloride; In 1-methyl-pyrrolidin-2-one; at 70 ℃; for 18h;

DOI:10.1016/j.bmc.2008.05.024

Reference yield: 38.0%

Glyoxal (131543-46-9,107-22-2) + 2-amino-3-({4-[2-(4-tert-butylphenyl)-1H-benzimidazol-4-yl]piperazin-1-yl}methyl)phenylamine (874279-71-7) → 5-({4-[2-(4-tert-butylphenyl)-1H-benzimidazol-4-yl]piperazin-1-yl}methyl)quinoxaline (874278-30-5)

Guidance literature:

In methanol; water; at 20 ℃; for 18h; Inert atmosphere;

DOI:10.1021/jm801572m

Reference yield:

2-amino-3-({4-[2-(4-tert-butylphenyl)-1H-benzimidazol-4-yl]piperazin-1-yl}methyl)phenylamine (874279-71-7) + 1,1'-Thiocarbonyldiimidazole (6160-65-2) → C29H32N6S (874278-26-9)

Guidance literature:

In tetrahydrofuran; at 60 ℃; for 2h;

DOI:10.1016/j.bmc.2008.05.024

upstream raw materials:

2-({4-[2-(4-tert-butylphenyl)-1H-benzo[d]imidazol-4-yl]piperazin-1-yl}methyl)-6-nitrophenylamine

Downstream raw materials:

C₂₉H₃₂N₆S

5-({4-[2-(4-tert-butylphenyl)-1H-benzimidazol-4-yl]piperazin-1-yl}methyl)quinoxaline

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