2,8-bis(4-hydroxyphenyl)-4,10-dimethyl-6H,12H-5,11-methanodibenzo[b,f]diazocine

Base Information

Chemical Name:2,8-bis(4-hydroxyphenyl)-4,10-dimethyl-6H,12H-5,11-methanodibenzo[b,f]diazocine
CAS No.:749257-29-2
Molecular Formula:C₂₉H₂₆N₂O₂
Molecular Weight:434.538
Hs Code.:

Synonyms:2,8-bis(4-hydroxyphenyl)-4,10-dimethyl-6H,12H-5,11-methanodibenzo[b,f]diazocine

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Chemical Property of 2,8-bis(4-hydroxyphenyl)-4,10-dimethyl-6H,12H-5,11-methanodibenzo[b,f]diazocine

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Technology Process of 2,8-bis(4-hydroxyphenyl)-4,10-dimethyl-6H,12H-5,11-methanodibenzo[b,f]diazocine

There total 3 articles about 2,8-bis(4-hydroxyphenyl)-4,10-dimethyl-6H,12H-5,11-methanodibenzo[b,f]diazocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 749257-26-9
2,8-bis(4-methoxyphenyl)-4,10-dimethyl-6H,12H-5,11-methanodibenzo[b,f]diazocine

: 749257-29-2
2,8-bis(4-hydroxyphenyl)-4,10-dimethyl-6H,12H-5,11-methanodibenzo[b,f]diazocine

Guidance literature:: With boron tribromide; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1055/s-2004-829117

Reference yield:

: 5720-07-0
4-methoxyphenylboronic acid

: 749257-29-2
2,8-bis(4-hydroxyphenyl)-4,10-dimethyl-6H,12H-5,11-methanodibenzo[b,f]diazocine

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / CsF / [Pd(P-t-Bu₃)2] / tetrahydrofuran / 6 h / 40 °C

2: 99 percent / BBr₃ / CH₂Cl₂ / 16 h / 20 °C

With boron tribromide; cesium fluoride; bis(tri-t-butylphosphine)palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; 1: Suzuki cross-coupling reaction;
DOI:10.1055/s-2004-829117

Reference yield:

: 390357-37-6
(rac)-2,8-diiodo-4,10-dimethyl-5,11-methano-6H,12H-dibenzo[b,f][1,5]diazocine

: 749257-29-2
2,8-bis(4-hydroxyphenyl)-4,10-dimethyl-6H,12H-5,11-methanodibenzo[b,f]diazocine

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / CsF / [Pd(P-t-Bu₃)2] / tetrahydrofuran / 6 h / 40 °C

2: 99 percent / BBr₃ / CH₂Cl₂ / 16 h / 20 °C

With boron tribromide; cesium fluoride; bis(tri-t-butylphosphine)palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; 1: Suzuki cross-coupling reaction;
DOI:10.1055/s-2004-829117