(2R,3R)-2,3-Bis-[(Z)-3-(4-methoxycarbonyloxy-phenyl)-acryloyloxy]-succinic acid

Base Information

Chemical Name:(2R,3R)-2,3-Bis-[(Z)-3-(4-methoxycarbonyloxy-phenyl)-acryloyloxy]-succinic acid
CAS No.:222320-75-4
Molecular Formula:C₂₆H₂₂O₁₄
Molecular Weight:558.452
Hs Code.:

Synonyms:(2R,3R)-2,3-Bis-[(Z)-3-(4-methoxycarbonyloxy-phenyl)-acryloyloxy]-succinic acid

Suppliers and Price of (2R,3R)-2,3-Bis-[(Z)-3-(4-methoxycarbonyloxy-phenyl)-acryloyloxy]-succinic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2R,3R)-2,3-Bis-[(Z)-3-(4-methoxycarbonyloxy-phenyl)-acryloyloxy]-succinic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2R,3R)-2,3-Bis-[(Z)-3-(4-methoxycarbonyloxy-phenyl)-acryloyloxy]-succinic acid

There total 4 articles about (2R,3R)-2,3-Bis-[(Z)-3-(4-methoxycarbonyloxy-phenyl)-acryloyloxy]-succinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1427216-41-8
C₅₂H₄₂O₁₄

: 222320-75-4
(2R,3R)-2,3-Bis-[(Z)-3-(4-methoxycarbonyloxy-phenyl)-acryloyloxy]-succinic acid

Guidance literature:: With methoxybenzene; trifluoroacetic acid; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmcl.2013.01.042

Reference yield:

: 7400-08-0,50940-26-6
para-coumaric acid

: 222320-75-4
(2R,3R)-2,3-Bis-[(Z)-3-(4-methoxycarbonyloxy-phenyl)-acryloyloxy]-succinic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1N aq. NaOH / 0 °C

2: oxalyl chloride / 1 h / Ambient temperature

3: 2.) 80 percent aq. HOAc / 1.) 135 - 160 deg C, 2.) reflux, 30 min

With sodium hydroxide; oxalyl dichloride; acetic acid;
DOI:10.1021/jm9804735