2-(3-methoxyphenyl)-1,1-dioxo-1λ⁶-thiomorpholine-4-carboxylic acid tert-butyl ester

Base Information

• Chemical Name: 2-(3-methoxyphenyl)-1,1-dioxo-1λ⁶-thiomorpholine-4-carboxylic acid tert-butyl ester
• CAS No.: 1598382-96-7
• Molecular Formula: C₁₆H₂₃NO₅S
• Molecular Weight: 341.428

Synonyms:2-(3-methoxyphenyl)-1,1-dioxo-1λ⁶-thiomorpholine-4-carboxylic acid tert-butyl ester

Chemical Property of 2-(3-methoxyphenyl)-1,1-dioxo-1λ⁶-thiomorpholine-4-carboxylic acid tert-butyl ester

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Technology Process of 2-(3-methoxyphenyl)-1,1-dioxo-1λ⁶-thiomorpholine-4-carboxylic acid tert-butyl ester

There total 5 articles about 2-(3-methoxyphenyl)-1,1-dioxo-1λ⁶-thiomorpholine-4-carboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl 2-(3-methoxyphenyl)thiomorpholine-4-carboxylate (1598382-95-6) → 2-(3-methoxyphenyl)-1,1-dioxo-1λ6-thiomorpholine-4-carboxylic acid tert-butyl ester (1598382-96-7)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 1.5h;

Reference yield:

2-(3-methoxyphenyl)-3-thiomorpholinone → 2-(3-methoxyphenyl)-1,1-dioxo-1λ6-thiomorpholine-4-carboxylic acid tert-butyl ester (1598382-96-7)

Guidance literature:

Multi-step reaction with 3 steps

1.1: acetic acid; sodium tetrahydroborate / 1,4-dioxane / 0 °C / Reflux

1.2: 20 °C

2.1: acetonitrile / 36 h / 20 °C

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1.5 h / 20 °C

With sodium tetrahydroborate; acetic acid; 3-chloro-benzenecarboperoxoic acid; In 1,4-dioxane; dichloromethane; acetonitrile;

Reference yield:

2-(3-methoxyphenyl)thiomorpholine (88788-99-2) → 2-(3-methoxyphenyl)-1,1-dioxo-1λ6-thiomorpholine-4-carboxylic acid tert-butyl ester (1598382-96-7)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / 36 h / 20 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1.5 h / 20 °C

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile;

upstream raw materials:

2-(3-methoxyphenyl)thiomorpholine

tert-butyl 2-(3-methoxyphenyl)thiomorpholine-4-carboxylate

methyl (3-methoxyphenyl)acetate

bromo-(3-methoxy-phenyl)-acetic acid methyl ester

Downstream raw materials:

2-(3-methoxyphenyl)thiomorpholine1,1-dioxide

(S)-1,1,1-trifluoro-3-[2-(3-methoxyphenyl)-1,1-dioxo-1λ⁶-thiomorpholin-4-yl]-propan-2-ol

(4-chlorophenyl)-carbamic acid (S)-2,2,2-trifluoro-1-[(R)-2-(3-methoxyphenyl)-1,1-dioxo-1λ⁶-thiomorpholin-4-ylmethyl]-ethyl ester

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