C₁₃⁽¹³⁾CH₁₃NO₂S

Base Information

Chemical Name:C₁₃⁽¹³⁾CH₁₃NO₂S
CAS No.:1311141-36-2
Molecular Formula:C₁₄H₁₃NO₂S
Molecular Weight:260.318
Hs Code.:

C<sub>13</sub><sup>(13)</sup>CH<sub>13</sub>NO<sub>2</sub>S

Synonyms:C₁₃⁽¹³⁾CH₁₃NO₂S

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Chemical Property of C₁₃⁽¹³⁾CH₁₃NO₂S

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Technology Process of C₁₃⁽¹³⁾CH₁₃NO₂S

There total 3 articles about C₁₃⁽¹³⁾CH₁₃NO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 10383-90-1
⁽¹³⁾C-benzaldehyde

: 70-55-3
toluene-4-sulfonamide

: 1311141-36-2
C₁₃⁽¹³⁾CH₁₃NO₂S

Guidance literature:: With amberlyst 15; In toluene; at 130 ℃; for 12h; Molecular sieve;
DOI:10.3762/bjoc.7.96

Reference yield:

: 54522-91-7
[α-13C]-benzyl alcohol

: 1311141-36-2
C₁₃⁽¹³⁾CH₁₃NO₂S

Guidance literature:: Multi-step reaction with 2 steps

1: Dess-Martin periodane / dichloromethane / 4 h / 20 °C

2: amberlyst 15 / toluene / 12 h / 130 °C / Molecular sieve

With Dess-Martin periodane; In dichloromethane; toluene;
DOI:10.3762/bjoc.7.96

Reference yield:

: 3880-99-7
1-(13C)benzoic acid

: 1311141-36-2
C₁₃⁽¹³⁾CH₁₃NO₂S

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / diethyl ether / 2.33 h / 0 - 50 °C

2: Dess-Martin periodane / dichloromethane / 4 h / 20 °C

3: amberlyst 15 / toluene / 12 h / 130 °C / Molecular sieve

With lithium aluminium tetrahydride; Dess-Martin periodane; In diethyl ether; dichloromethane; toluene;
DOI:10.3762/bjoc.7.96