E-2-methyl-1-phenylhept-6-en-1-one dimethylhydrazone

Base Information

• Chemical Name: E-2-methyl-1-phenylhept-6-en-1-one dimethylhydrazone
• CAS No.: 224426-58-8
• Molecular Formula: C₁₆H₂₄N₂
• Molecular Weight: 244.38
• Mol file: 224426-58-8.mol

Synonyms:E-2-methyl-1-phenylhept-6-en-1-one dimethylhydrazone

Chemical Property of E-2-methyl-1-phenylhept-6-en-1-one dimethylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of E-2-methyl-1-phenylhept-6-en-1-one dimethylhydrazone

There total 6 articles about E-2-methyl-1-phenylhept-6-en-1-one dimethylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bromopentene (1119-51-3) → E-2-methyl-1-phenylhept-6-en-1-one dimethylhydrazone (224426-58-8)

Guidance literature:

Multi-step reaction with 3 steps

1: NaI / acetone

2: (i) NaH, DMSO, (ii) /BRN= 1736871/

3: AcOH, NaOAc, MgSO₄

With sodium acetate; magnesium sulfate; acetic acid; sodium iodide; In acetone;

DOI:10.1021/ja00448a031

Reference yield:

1-iodo-4-pentene (7766-48-5) → E-2-methyl-1-phenylhept-6-en-1-one dimethylhydrazone (224426-58-8)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) NaH, DMSO, (ii) /BRN= 1736871/

2: AcOH, NaOAc, MgSO₄

With sodium acetate; magnesium sulfate; acetic acid;

DOI:10.1021/ja00448a031

Reference yield:

2-methyl-1-phenylhept-6-en-1-one (15775-35-6) + N,N-Dimethylhydrazine (57-14-7) → E-2-methyl-1-phenylhept-6-en-1-one dimethylhydrazone (224426-58-8)

Guidance literature:

With sodium acetate; magnesium sulfate; acetic acid;

DOI:10.1021/ja00448a031

upstream raw materials:

2-methyl-1-phenylhept-6-en-1-one

N,N-Dimethylhydrazine

propiophenone N,N-dimethylhydrazone

bromopentene

Downstream raw materials:

2-methyl-1-phenylhept-6-en-1-one

1-phenyl-2-methyl-6,7-epoxyheptan-1-one