[2-((1R,6R)-6-tert-Butoxycarbonylamino-3-methoxycarbonyl-cyclohexa-2,4-dienyloxy)-2,2-bis-methoxycarbonyl-ethyl]-trimethyl-ammonium; iodide

Base Information

Chemical Name:[2-((1R,6R)-6-tert-Butoxycarbonylamino-3-methoxycarbonyl-cyclohexa-2,4-dienyloxy)-2,2-bis-methoxycarbonyl-ethyl]-trimethyl-ammonium; iodide
CAS No.:97279-86-2
Molecular Formula:C₂₂H₃₅N₂O₉*I
Molecular Weight:598.432
Hs Code.:

[2-((1R,6R)-6-tert-Butoxycarbonylamino-3-methoxycarbonyl-cyclohexa-2,4-dienyloxy)-2,2-bis-methoxycarbonyl-ethyl]-trimethyl-ammonium; iodide

Synonyms:[2-((1R,6R)-6-tert-Butoxycarbonylamino-3-methoxycarbonyl-cyclohexa-2,4-dienyloxy)-2,2-bis-methoxycarbonyl-ethyl]-trimethyl-ammonium; iodide

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Chemical Property of [2-((1R,6R)-6-tert-Butoxycarbonylamino-3-methoxycarbonyl-cyclohexa-2,4-dienyloxy)-2,2-bis-methoxycarbonyl-ethyl]-trimethyl-ammonium; iodide

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Technology Process of [2-((1R,6R)-6-tert-Butoxycarbonylamino-3-methoxycarbonyl-cyclohexa-2,4-dienyloxy)-2,2-bis-methoxycarbonyl-ethyl]-trimethyl-ammonium; iodide

There total 4 articles about [2-((1R,6R)-6-tert-Butoxycarbonylamino-3-methoxycarbonyl-cyclohexa-2,4-dienyloxy)-2,2-bis-methoxycarbonyl-ethyl]-trimethyl-ammonium; iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-Diazenyl-malonic acid dimethyl ester

: 97279-86-2
[2-((1R,6R)-6-tert-Butoxycarbonylamino-3-methoxycarbonyl-cyclohexa-2,4-dienyloxy)-2,2-bis-methoxycarbonyl-ethyl]-trimethyl-ammonium; iodide

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / Rh₂(OAc)4 / benzene / 70 °C

2: 94 percent / Et₃N / CH₂Cl₂ / Ambient temperature

3: CH₂Cl₂ / Ambient temperature

With dirhodium tetraacetate; triethylamine; In dichloromethane; benzene;
DOI:10.1021/ja00303a038

Reference yield:

: 97279-83-9
(3R,4R)-4-tert-Butoxycarbonylamino-3-hydroxy-cyclohexa-1,5-dienecarboxylic acid methyl ester

: 97279-86-2
[2-((1R,6R)-6-tert-Butoxycarbonylamino-3-methoxycarbonyl-cyclohexa-2,4-dienyloxy)-2,2-bis-methoxycarbonyl-ethyl]-trimethyl-ammonium; iodide

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / Rh₂(OAc)4 / benzene / 70 °C

2: 94 percent / Et₃N / CH₂Cl₂ / Ambient temperature

3: CH₂Cl₂ / Ambient temperature

With dirhodium tetraacetate; triethylamine; In dichloromethane; benzene;
DOI:10.1021/ja00303a038

Reference yield:

: 97279-84-0
2-((1S,6S)-6-tert-Butoxycarbonylamino-3-methoxycarbonyl-cyclohexa-2,4-dienyloxy)-malonic acid dimethyl ester

: 97279-86-2
[2-((1R,6R)-6-tert-Butoxycarbonylamino-3-methoxycarbonyl-cyclohexa-2,4-dienyloxy)-2,2-bis-methoxycarbonyl-ethyl]-trimethyl-ammonium; iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / Et₃N / CH₂Cl₂ / Ambient temperature

2: CH₂Cl₂ / Ambient temperature

With triethylamine; In dichloromethane;
DOI:10.1021/ja00303a038