[10,20-bis(3,5-di-n-tridecylphenyl)-5-(4-acetyl-phenyl)porphyrinato(2-)-κN21,κN22,κN23,κN24] zinc(II)

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Chemical Name:[10,20-bis(3,5-di-n-tridecylphenyl)-5-(4-acetyl-phenyl)porphyrinato(2-)-κN21,κN22,κN23,κN24] zinc(II)
CAS No.:1312229-58-5
Molecular Formula:C₉₂H₁₃₀N₄OZn
Molecular Weight:1373.46
Hs Code.:

Synonyms:[10,20-bis(3,5-di-n-tridecylphenyl)-5-(4-acetyl-phenyl)porphyrinato(2-)-κN21,κN22,κN23,κN24] zinc(II)

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Chemical Property of [10,20-bis(3,5-di-n-tridecylphenyl)-5-(4-acetyl-phenyl)porphyrinato(2-)-κN21,κN22,κN23,κN24] zinc(II)

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Technology Process of [10,20-bis(3,5-di-n-tridecylphenyl)-5-(4-acetyl-phenyl)porphyrinato(2-)-κN21,κN22,κN23,κN24] zinc(II)

There total 1 articles about [10,20-bis(3,5-di-n-tridecylphenyl)-5-(4-acetyl-phenyl)porphyrinato(2-)-κN21,κN22,κN23,κN24] zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1312229-53-0
[5,15-bis(3,5-di-n-tridecylphenyl)-porphyrinato(2-)-κN21,κN22,κN23,κN24] zinc(II)

: 171364-81-1
1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethanone

: 1312229-58-5
[10,20-bis(3,5-di-n-tridecylphenyl)-5-(4-acetyl-phenyl)porphyrinato(2-)-κN21,κN22,κN23,κN24] zinc(II)

: 1312229-60-9
[5,15-bis(4-acetyl-phenyl)-10,20-bis(3,5-di-n-tridecylphenyl)porphyrinato(2-)-κN21,κN22,κN23,κN24] zinc(II)

Guidance literature:: [5,15-bis(3,5-di-n-tridecylphenyl)-porphyrinato(2-)-κN21,κN22,κN23,κN24] zinc(II); With pyridine; N-Bromosuccinimide; In dichloromethane; at 0 ℃; for 0.166667h; Inert atmosphere;

1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethanone; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In dichloromethane; toluene; for 16.6667h; Inert atmosphere; Reflux; Sonication;
DOI:10.1021/cm2004648

Reference yield: 60.0%

: 1312229-58-5
[10,20-bis(3,5-di-n-tridecylphenyl)-5-(4-acetyl-phenyl)porphyrinato(2-)-κN21,κN22,κN23,κN24] zinc(II)

: {μ-[10,10'-Bis(4-acetylphenyl)-5,5',15,15'-tetrakis(3,5-di-n-tridecylphenyl)-18,18':20,20'-dicyclo-2,2'-biporphyrinato(4-)-κN21,κN22,κN23,κN24:κN210,κN220,κN230,κN240]} dizinc(II)

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; scandium tris(trifluoromethanesulfonate); In toluene; at 80 ℃; for 3h; Inert atmosphere;
DOI:10.1021/cm2004648