3-[2'-fluoro-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol

Base Information

Chemical Name:3-[2'-fluoro-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol
CAS No.:1560987-51-0
Molecular Formula:C₁₅H₉FN₄S₂
Molecular Weight:328.394
Hs Code.:

Synonyms:3-[2'-fluoro-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol

Suppliers and Price of 3-[2'-fluoro-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-[2'-fluoro-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-[2'-fluoro-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol

There total 1 articles about 3-[2'-fluoro-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1253043-54-7
C₁₄H₉FN₂OS

: 1560987-51-0
3-[2'-fluoro-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 6 h / Reflux

2: potassium hydroxide / ethanol / 4 h / Reflux

With hydrazine hydrate; potassium hydroxide; In ethanol;
DOI:10.1007/s00044-014-0944-x

Reference yield: 83.0%

: 462-72-6
4-bromo-1-fluorobutane

: 1560987-51-0
3-[2'-fluoro-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol

: 1560987-61-2
3-[2'-fluoro-(1,1'-biphenyl)-3-yl]-6-[(4-fluorobutyl)sulfanyl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 0.0833333h; Temperature; Microwave irradiation;
DOI:10.1007/s00044-014-0944-x

Reference yield: 82.0%

: 1560987-51-0
3-[2'-fluoro-(1,1'-biphenyl)-3-yl][1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6-thiol

: 5332-06-9
4-bromobutanenitrile

: 1560987-64-5
4-{[3-(2'-fluoro-(1,1'-biphenyl)-3-yl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-6-yl]sulfanyl}butanenitrile

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 0.0833333h; Temperature; Microwave irradiation;
DOI:10.1007/s00044-014-0944-x