3-N'-hydroxyamidinobenzyl 2,6-dichloro-4-N'-hydroxyamidinophenyl ether

Base Information

Chemical Name:3-N'-hydroxyamidinobenzyl 2,6-dichloro-4-N'-hydroxyamidinophenyl ether
CAS No.:1456777-94-8
Molecular Formula:C₁₅H₁₄Cl₂N₄O₃
Molecular Weight:369.207
Hs Code.:

Synonyms:3-N'-hydroxyamidinobenzyl 2,6-dichloro-4-N'-hydroxyamidinophenyl ether

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Chemical Property of 3-N'-hydroxyamidinobenzyl 2,6-dichloro-4-N'-hydroxyamidinophenyl ether

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Technology Process of 3-N'-hydroxyamidinobenzyl 2,6-dichloro-4-N'-hydroxyamidinophenyl ether

There total 3 articles about 3-N'-hydroxyamidinobenzyl 2,6-dichloro-4-N'-hydroxyamidinophenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1456777-73-3
3-cyanobenzyl 4-cyano-2,6-dichlorophenyl ether

: 1456777-94-8
3-N'-hydroxyamidinobenzyl 2,6-dichloro-4-N'-hydroxyamidinophenyl ether

Guidance literature:: With hydroxylamine hydrochloride; potassium tert-butylate; In dimethyl sulfoxide;
DOI:10.1016/j.ejmech.2013.06.033

Reference yield:

: 1891-95-8
chloroxynil

: 1456777-94-8
3-N'-hydroxyamidinobenzyl 2,6-dichloro-4-N'-hydroxyamidinophenyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 70 - 80 °C

1.2: 60 h / 20 °C

2.1: hydroxylamine hydrochloride; potassium tert-butylate / dimethyl sulfoxide

With hydroxylamine hydrochloride; potassium tert-butylate; potassium carbonate; In dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2013.06.033

Reference yield:

: 28188-41-2
m-(bromomethyl)benzonitrile

: 1456777-94-8
3-N'-hydroxyamidinobenzyl 2,6-dichloro-4-N'-hydroxyamidinophenyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 70 - 80 °C

1.2: 60 h / 20 °C

2.1: hydroxylamine hydrochloride; potassium tert-butylate / dimethyl sulfoxide

With hydroxylamine hydrochloride; potassium tert-butylate; potassium carbonate; In dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2013.06.033