1,8-[N,N'-bis((3-formyl-2-hydroxy-5-methyl)benzyl)]-4,11-dimethyl-1,4,8,11-tetraaza-5,5,7,12,12,14-hexamethylcyclotetradecane

Base Information

Chemical Name:1,8-[N,N'-bis((3-formyl-2-hydroxy-5-methyl)benzyl)]-4,11-dimethyl-1,4,8,11-tetraaza-5,5,7,12,12,14-hexamethylcyclotetradecane
CAS No.:741253-47-4
Molecular Formula:C₃₆H₅₆N₄O₄
Molecular Weight:608.865
Hs Code.:

Synonyms:1,8-[N,N'-bis((3-formyl-2-hydroxy-5-methyl)benzyl)]-4,11-dimethyl-1,4,8,11-tetraaza-5,5,7,12,12,14-hexamethylcyclotetradecane

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Chemical Property of 1,8-[N,N'-bis((3-formyl-2-hydroxy-5-methyl)benzyl)]-4,11-dimethyl-1,4,8,11-tetraaza-5,5,7,12,12,14-hexamethylcyclotetradecane

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Technology Process of 1,8-[N,N'-bis((3-formyl-2-hydroxy-5-methyl)benzyl)]-4,11-dimethyl-1,4,8,11-tetraaza-5,5,7,12,12,14-hexamethylcyclotetradecane

There total 3 articles about 1,8-[N,N'-bis((3-formyl-2-hydroxy-5-methyl)benzyl)]-4,11-dimethyl-1,4,8,11-tetraaza-5,5,7,12,12,14-hexamethylcyclotetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1,8-[N,N'-bis(3-formyl-2-hydroxy-5-methyl)benzyl]-1,8-diazania-4,11-diazatricyclo[9.3.1.1^4,8]-5,5,7,12,12,14-hexamethylhexadecane dichloride

: 741253-47-4
1,8-[N,N'-bis((3-formyl-2-hydroxy-5-methyl)benzyl)]-4,11-dimethyl-1,4,8,11-tetraaza-5,5,7,12,12,14-hexamethylcyclotetradecane

Guidance literature:: With sodium tetrahydroborate; In methanol; water; for 3h; Heating;
DOI:10.1246/bcsj.77.1153

Reference yield:

: 5,7,7,12,14,14-hexamethyl-1,4,8,11-tetraazatricyclo{9.3.1.1(4,8)}hexadecane

: 741253-47-4
1,8-[N,N'-bis((3-formyl-2-hydroxy-5-methyl)benzyl)]-4,11-dimethyl-1,4,8,11-tetraaza-5,5,7,12,12,14-hexamethylcyclotetradecane

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / acetonitrile / 72 h / 25 °C

2: 73 percent / NaBH₄ / methanol; H₂O / 3 h / Heating

With sodium tetrahydroborate; In methanol; water; acetonitrile;
DOI:10.1246/bcsj.77.1153

Reference yield:

: 192819-68-4
3-chloromethyl-5-methylsalicylaldehyde

: 741253-47-4
1,8-[N,N'-bis((3-formyl-2-hydroxy-5-methyl)benzyl)]-4,11-dimethyl-1,4,8,11-tetraaza-5,5,7,12,12,14-hexamethylcyclotetradecane

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / acetonitrile / 72 h / 25 °C

2: 73 percent / NaBH₄ / methanol; H₂O / 3 h / Heating

With sodium tetrahydroborate; In methanol; water; acetonitrile;
DOI:10.1246/bcsj.77.1153