C₆₅H₅₉N₃S₄Se₃

Base Information

• Chemical Name: C₆₅H₅₉N₃S₄Se₃
• CAS No.: 1185741-67-6
• Molecular Formula: C₆₅H₅₉N₃S₄Se₃
• Molecular Weight: 1247.35
• Mol file: 1185741-67-6.mol

Synonyms:C₆₅H₅₉N₃S₄Se₃

Chemical Property of C₆₅H₅₉N₃S₄Se₃

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₆₅H₅₉N₃S₄Se₃

There total 2 articles about C₆₅H₅₉N₃S₄Se₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C80H104O3S4Si3 (1185741-76-7) → C65H59N3S4Se3 (1185741-67-6)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

2: carbon tetrabromide; triphenylphosphine / dichloromethane / 20 °C

3: tetrahydrofuran / 20 °C

With carbon tetrabromide; tetrabutyl ammonium fluoride; triphenylphosphine; In tetrahydrofuran; dichloromethane;

DOI:10.1039/b906286f

Reference yield:

C62H59Br3S4 (1227007-64-8) + potassium selenocyanate (3425-46-5) → C65H59N3S4Se3 (1185741-67-6)

Guidance literature:

In tetrahydrofuran; at 20 ℃;

DOI:10.1039/b906286f

Reference yield: 74.0%

C65H59N3S4Se3 (1185741-67-6) + acetic anhydride (108-24-7) → C68H68O3S4Se3 (1185741-77-8)

Guidance literature:

C₆₅H₅₉N₃S₄Se₃; With lithium triethylborohydride; In tetrahydrofuran; at -78 ℃;

acetic anhydride; In tetrahydrofuran; at -78 ℃;

DOI:10.1039/b906286f

upstream raw materials:

C₈₀H₁₀₄O₃S₄Si₃

C₆₂H₅₉Br₃S₄

potassium selenocyanate

Downstream raw materials:

C₆₂H₆₂S₄Se₃

C₆₈H₆₈O₃S₄Se₃