(S)-(Z)-N-(benzyloxycarbonyl)-4-aminohex-2-enedioic acid, 6-benzyl ester

Base Information

Chemical Name:(S)-(Z)-N-(benzyloxycarbonyl)-4-aminohex-2-enedioic acid, 6-benzyl ester
CAS No.:142955-57-5
Molecular Formula:C₂₁H₂₁NO₆
Molecular Weight:383.401
Hs Code.:

Synonyms:(S)-(Z)-N-(benzyloxycarbonyl)-4-aminohex-2-enedioic acid, 6-benzyl ester

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Chemical Property of (S)-(Z)-N-(benzyloxycarbonyl)-4-aminohex-2-enedioic acid, 6-benzyl ester

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Technology Process of (S)-(Z)-N-(benzyloxycarbonyl)-4-aminohex-2-enedioic acid, 6-benzyl ester

There total 9 articles about (S)-(Z)-N-(benzyloxycarbonyl)-4-aminohex-2-enedioic acid, 6-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 171626-96-3
(S)-(Z)-N-(benzyloxycarbonyl)-4-aminohex-2-enedioic acid, 1-tert-butyl 6-benzyl diester

: 142955-57-5
(S)-(Z)-N-(benzyloxycarbonyl)-4-aminohex-2-enedioic acid, 6-benzyl ester

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 2h; 0 deg C -> RT;
DOI:10.1016/0040-4020(95)00776-5

Reference yield:

: 133565-44-3
N-benzyloxycarbonyl (S)-β-homoserine benzyl ester

: 142955-57-5
(S)-(Z)-N-(benzyloxycarbonyl)-4-aminohex-2-enedioic acid, 6-benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / pyridine*sulphur trioxide, triethylamine / dimethylsulfoxide / 0.33 h / Ambient temperature

2: 38 percent / benzoic acid / methanol / 72 h / -20 °C

3: 87 percent / trifluoroacetic acid / CH₂Cl₂ / 2 h / 0 deg C -> RT

With sulfur trioxide pyridine complex; triethylamine; benzoic acid; trifluoroacetic acid; In methanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1016/0040-4020(95)00776-5

Reference yield:

: 142955-59-7
(S)-3-Benzyloxycarbonylamino-4-oxo-butyric acid benzyl ester

: 142955-57-5
(S)-(Z)-N-(benzyloxycarbonyl)-4-aminohex-2-enedioic acid, 6-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 38 percent / benzoic acid / methanol / 72 h / -20 °C

2: 87 percent / trifluoroacetic acid / CH₂Cl₂ / 2 h / 0 deg C -> RT

With benzoic acid; trifluoroacetic acid; In methanol; dichloromethane;
DOI:10.1016/0040-4020(95)00776-5