(S)-(Z)-N-(benzyloxycarbonyl)-4-aminohex-2-enedioic acid, 1-tert-butyl 6-benzyl diester

Base Information

Chemical Name:(S)-(Z)-N-(benzyloxycarbonyl)-4-aminohex-2-enedioic acid, 1-tert-butyl 6-benzyl diester
CAS No.:171626-96-3
Molecular Formula:C₂₅H₂₉NO₆
Molecular Weight:439.508
Hs Code.:

Synonyms:(S)-(Z)-N-(benzyloxycarbonyl)-4-aminohex-2-enedioic acid, 1-tert-butyl 6-benzyl diester

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Chemical Property of (S)-(Z)-N-(benzyloxycarbonyl)-4-aminohex-2-enedioic acid, 1-tert-butyl 6-benzyl diester

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Technology Process of (S)-(Z)-N-(benzyloxycarbonyl)-4-aminohex-2-enedioic acid, 1-tert-butyl 6-benzyl diester

There total 2 articles about (S)-(Z)-N-(benzyloxycarbonyl)-4-aminohex-2-enedioic acid, 1-tert-butyl 6-benzyl diester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 86302-43-4,35000-38-5
(tert-Butoxycarbonylmethylene)triphenylphosphorane

: 142955-59-7
(S)-3-Benzyloxycarbonylamino-4-oxo-butyric acid benzyl ester

: 171626-96-3
(S)-(Z)-N-(benzyloxycarbonyl)-4-aminohex-2-enedioic acid, 1-tert-butyl 6-benzyl diester

: (S)-(E)-N-(benzyloxycarbonyl)-4-aminohex-2-enedioic acid, 1-tert-butyl 6-benzyl diester

Guidance literature:: With benzoic acid; In methanol; at -20 ℃; for 72h;
DOI:10.1016/0040-4020(95)00776-5

Reference yield:

: 133565-44-3
N-benzyloxycarbonyl (S)-β-homoserine benzyl ester

: 171626-96-3
(S)-(Z)-N-(benzyloxycarbonyl)-4-aminohex-2-enedioic acid, 1-tert-butyl 6-benzyl diester

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / pyridine*sulphur trioxide, triethylamine / dimethylsulfoxide / 0.33 h / Ambient temperature

2: 38 percent / benzoic acid / methanol / 72 h / -20 °C

With sulfur trioxide pyridine complex; triethylamine; benzoic acid; In methanol; dimethyl sulfoxide;
DOI:10.1016/0040-4020(95)00776-5