(Z)-5a,6,7,9a-Tetrahydro-5a,6-tetramethylene-11-[ethoxycarbonyl(nitro)methylene]naphtho[1',2':4,5]imidazo[1,2-a]pyridine

Base Information

• Chemical Name: (Z)-5a,6,7,9a-Tetrahydro-5a,6-tetramethylene-11-[ethoxycarbonyl(nitro)methylene]naphtho[1',2':4,5]imidazo[1,2-a]pyridine
• CAS No.: 234762-41-5
• Molecular Formula: C₃₅H₃₁N₃O₄
• Molecular Weight: 557.649
• Mol file: 234762-41-5.mol

Synonyms:(Z)-5a,6,7,9a-Tetrahydro-5a,6-tetramethylene-11-[ethoxycarbonyl(nitro)methylene]naphtho[1',2':4,5]imidazo[1,2-a]pyridine

Chemical Property of (Z)-5a,6,7,9a-Tetrahydro-5a,6-tetramethylene-11-[ethoxycarbonyl(nitro)methylene]naphtho[1',2':4,5]imidazo[1,2-a]pyridine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Z)-5a,6,7,9a-Tetrahydro-5a,6-tetramethylene-11-[ethoxycarbonyl(nitro)methylene]naphtho[1',2':4,5]imidazo[1,2-a]pyridine

There total 1 articles about (Z)-5a,6,7,9a-Tetrahydro-5a,6-tetramethylene-11-[ethoxycarbonyl(nitro)methylene]naphtho[1',2':4,5]imidazo[1,2-a]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

nitroacetic acid ethyl ester (626-35-7) + 5a,6,7,9a-Tetrahydro-5,6-tetramethylene-7,9-diphenyl-5H-naphtho[1',2':4,5]imidazo[1,2-a]pyridine (138792-73-1) → (E)-5a,6,7,9a-Tetrahydro-5a,6-tetramethylene-11-[ethoxycarbonyl(nitro)methylene]naphtho[1',2':4,5]imidazo[1,2-a]pyridine (234762-40-4) + (Z)-5a,6,7,9a-Tetrahydro-5a,6-tetramethylene-11-[ethoxycarbonyl(nitro)methylene]naphtho[1',2':4,5]imidazo[1,2-a]pyridine (234762-41-5)

Guidance literature:

With manganese(IV) oxide; In acetone; for 0.75h;

Reference yield: 100.0%

1H-indene-1,3(2H)-dione (606-23-5) + (Z)-5a,6,7,9a-Tetrahydro-5a,6-tetramethylene-11-[ethoxycarbonyl(nitro)methylene]naphtho[1',2':4,5]imidazo[1,2-a]pyridine (234762-41-5) → C40H30N2O2

Guidance literature:

With sodium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

Reference yield: 100.0%

(Z)-5a,6,7,9a-Tetrahydro-5a,6-tetramethylene-11-[ethoxycarbonyl(nitro)methylene]naphtho[1',2':4,5]imidazo[1,2-a]pyridine (234762-41-5) + cyanoacetic acid amide (107-91-5) → C34H28N4O

Guidance literature:

With sodium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

upstream raw materials:

nitroacetic acid ethyl ester

5a,6,7,9a-Tetrahydro-5,6-tetramethylene-7,9-diphenyl-5H-naphtho[1',2':4,5]imidazo[1,2-a]pyridine

Downstream raw materials:

C₃₄H₂₆N₄

(E)-5a,6,7,9a-Tetrahydro-5a,6-tetramethylene-11-[ethoxycarbonyl(nitro)methylene]naphtho[1',2':4,5]imidazo[1,2-a]pyridine