Technology Process of C52H79N5O7Si
There total 11 articles about C52H79N5O7Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C41H63N3O8Si; N-[(2S)-2-amino-3-phenylpropyl]-N,N-dimethylamine;
With
O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine;
In
N,N-dimethyl-formamide;
for 4h;
N-[(2S)-2-amino-3-phenylpropyl]-N,N-dimethylamine;
In
dichloromethane;
at 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation
1.2: 2 h
2.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 20 °C
3.1: trimethylaluminum / hexane; dichloromethane / 0.25 h
3.2: 20 °C
3.3: 2 h
4.1: potassium acetate; caesium carbonate / dimethyl sulfoxide / 0.02 h
4.2: 2 h / 60 °C
5.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 4 h
5.2: 2 h / 20 °C
With
titanium(IV) isopropylate; trimethylaluminum; potassium acetate; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; pyridine hydrogenfluoride; triethylamine;
In
tetrahydrofuran; pyridine; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: benzene / Heating / reflux
2.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation
2.2: 2 h
3.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 20 °C
4.1: trimethylaluminum / hexane; dichloromethane / 0.25 h
4.2: 20 °C
4.3: 2 h
5.1: potassium acetate; caesium carbonate / dimethyl sulfoxide / 0.02 h
5.2: 2 h / 60 °C
6.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 4 h
6.2: 2 h / 20 °C
With
titanium(IV) isopropylate; trimethylaluminum; potassium acetate; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; pyridine hydrogenfluoride; triethylamine;
In
tetrahydrofuran; pyridine; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; benzene;
