2-((Z)-2-(2-chlorostyryl)-5-nitro-1H-imidazol-1-yl)ethyl 2,3-dihydro-1,4-benzodioxine-5-carboxylate

Base Information

Chemical Name:2-((Z)-2-(2-chlorostyryl)-5-nitro-1H-imidazol-1-yl)ethyl 2,3-dihydro-1,4-benzodioxine-5-carboxylate
CAS No.:1609583-99-4
Molecular Formula:C₂₂H₁₈ClN₃O₆
Molecular Weight:455.854
Hs Code.:

Synonyms:2-((Z)-2-(2-chlorostyryl)-5-nitro-1H-imidazol-1-yl)ethyl 2,3-dihydro-1,4-benzodioxine-5-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-((Z)-2-(2-chlorostyryl)-5-nitro-1H-imidazol-1-yl)ethyl 2,3-dihydro-1,4-benzodioxine-5-carboxylate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-((Z)-2-(2-chlorostyryl)-5-nitro-1H-imidazol-1-yl)ethyl 2,3-dihydro-1,4-benzodioxine-5-carboxylate

There total 9 articles about 2-((Z)-2-(2-chlorostyryl)-5-nitro-1H-imidazol-1-yl)ethyl 2,3-dihydro-1,4-benzodioxine-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1609584-70-4
C₁₅H₁₅N₃O₆

: 89-98-5
2-chloro-benzaldehyde

: 1609583-99-4
2-((Z)-2-(2-chlorostyryl)-5-nitro-1H-imidazol-1-yl)ethyl 2,3-dihydro-1,4-benzodioxine-5-carboxylate

Guidance literature:: With sodium hydroxide; In methanol; dimethyl sulfoxide; at 20 ℃;
DOI:10.1016/j.bmc.2014.04.005

Reference yield:

: 4442-53-9
2,3-dihydro-1,4-benzodioxine-5-carboxylic acid

: 1609584-52-2
2-(2-((Z)-2-chlorostyryl)-5-nitro-1H-imidazol-1-yl)ethyl 4-methylbenzenesulfonate

: 1609583-99-4
2-((Z)-2-(2-chlorostyryl)-5-nitro-1H-imidazol-1-yl)ethyl 2,3-dihydro-1,4-benzodioxine-5-carboxylate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2014.04.005

Reference yield:

: 2411-83-8
methyl-2,3-dihydroxybenzoate

: 1609583-99-4
2-((Z)-2-(2-chlorostyryl)-5-nitro-1H-imidazol-1-yl)ethyl 2,3-dihydro-1,4-benzodioxine-5-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 70 °C / Inert atmosphere

2: methanol; sodium hydroxide / water; tetrahydrofuran / 2 h / 75 °C

3: potassium carbonate / N,N-dimethyl-formamide

With methanol; potassium carbonate; sodium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmc.2014.04.005