2-Benzyl-1,2,3,4,5,6,7,8-octahydro-1-(2,5-dimethyl-3-thienyl)-isochinolin

Base Information

Chemical Name:2-Benzyl-1,2,3,4,5,6,7,8-octahydro-1-(2,5-dimethyl-3-thienyl)-isochinolin
CAS No.:98237-63-9
Molecular Formula:C₂₃H₂₉NS
Molecular Weight:351.556
Hs Code.:

Synonyms:2-Benzyl-1,2,3,4,5,6,7,8-octahydro-1-(2,5-dimethyl-3-thienyl)-isochinolin

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Chemical Property of 2-Benzyl-1,2,3,4,5,6,7,8-octahydro-1-(2,5-dimethyl-3-thienyl)-isochinolin

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Technology Process of 2-Benzyl-1,2,3,4,5,6,7,8-octahydro-1-(2,5-dimethyl-3-thienyl)-isochinolin

There total 5 articles about 2-Benzyl-1,2,3,4,5,6,7,8-octahydro-1-(2,5-dimethyl-3-thienyl)-isochinolin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 100-39-0
benzyl bromide

: 98237-61-7
1-(2,5-Dimethyl-3-thienyl)-1,2,3,4,5,6,7,8-octahydro-isochinolin

: 98237-63-9
2-Benzyl-1,2,3,4,5,6,7,8-octahydro-1-(2,5-dimethyl-3-thienyl)-isochinolin

Guidance literature:: With potassium carbonate; potassium iodide; In benzene; for 15h; Heating;
DOI:10.1007/BF00798462

Reference yield:

: 26421-36-3
2,5-Dimethylthiophen-3-ylacetic acid chloride

: 98237-63-9
2-Benzyl-1,2,3,4,5,6,7,8-octahydro-1-(2,5-dimethyl-3-thienyl)-isochinolin

Guidance literature:: Multi-step reaction with 4 steps

1: 94.7 percent / K₂CO₃ / benzene / 2 h / Ambient temperature

2: P₂O₅ / benzene / 1.5 h / Heating

3: 4.9 g / NaBH₄ / ethanol; H₂O / 1 h / Ambient temperature

4: 97 percent / K₂CO₃, KI / benzene / 15 h / Heating

With sodium tetrahydroborate; phosphorus pentoxide; potassium carbonate; potassium iodide; In ethanol; water; benzene;
DOI:10.1007/BF00798462

Reference yield:

: 1-(2,5-Dimethyl-thiophen-3-ylmethyl)-3,4,5,6,7,8-hexahydro-isoquinoline

: 98237-63-9
2-Benzyl-1,2,3,4,5,6,7,8-octahydro-1-(2,5-dimethyl-3-thienyl)-isochinolin

Guidance literature:: Multi-step reaction with 2 steps

1: 4.9 g / NaBH₄ / ethanol; H₂O / 1 h / Ambient temperature

2: 97 percent / K₂CO₃, KI / benzene / 15 h / Heating

With sodium tetrahydroborate; potassium carbonate; potassium iodide; In ethanol; water; benzene;
DOI:10.1007/BF00798462