C₄₅H₄₂O₁₀

Base Information

Chemical Name:C₄₅H₄₂O₁₀
CAS No.:1229578-69-1
Molecular Formula:C₄₅H₄₂O₁₀
Molecular Weight:742.822
Hs Code.:

C<sub>45</sub>H<sub>42</sub>O<sub>10</sub>

Synonyms:C₄₅H₄₂O₁₀

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Chemical Property of C₄₅H₄₂O₁₀

Chemical Property:

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Technology Process of C₄₅H₄₂O₁₀

There total 13 articles about C₄₅H₄₂O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1229578-62-4
3-iodo-5-methoxy-8,8-dimethyl-8H-pyrano[3,2-g]chromone

: 1229578-63-5
1-(4,4,5,5-tetramethyl-1,3,2-dioxaborol-2-yl)-2,4,5-tris(p-methoxybenzyloxy)benzene

: 1229578-69-1
C₄₅H₄₂O₁₀

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate; In tetrahydrofuran; water; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.03.092

Reference yield:

: 31721-94-5
5,7-dihydroxy-chromen-4-one

: 1229578-69-1
C₄₅H₄₂O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1.1: calcium hydroxide / methanol / 72 h / 20 °C

2.1: potassium carbonate / acetone / 0.17 h / Cooling with ice

2.2: 3 h / Inert atmosphere; Reflux

3.1: methanol / 2 h / Reflux

4.1: pyridine; iodine / dichloromethane / 20 °C

5.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water / 20 °C / Inert atmosphere

With pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; iodine; sodium carbonate; potassium carbonate; calcium hydroxide; In methanol; dichloromethane; water; acetone; 5.1: |Suzuki-Miyaura Coupling;
DOI:10.1002/ejoc.201201339

Reference yield:

: 480-66-0,67471-34-5
2,4,6-trihydroxyacetophenone

: 1229578-69-1
C₄₅H₄₂O₁₀

Guidance literature:: Multi-step reaction with 6 steps

1.1: boron trifluoride diethyl etherate; methanesulfonyl chloride / 3.83 h / 20 - 90 °C

2.1: calcium hydroxide / methanol / 72 h / 20 °C

3.1: potassium carbonate / acetone / 0.17 h / Cooling with ice

3.2: 3 h / Inert atmosphere; Reflux

4.1: methanol / 2 h / Reflux

5.1: pyridine; iodine / dichloromethane / 20 °C

6.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water / 20 °C / Inert atmosphere

With pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; boron trifluoride diethyl etherate; iodine; sodium carbonate; potassium carbonate; methanesulfonyl chloride; calcium hydroxide; In methanol; dichloromethane; water; acetone; 1.1: |Vilsmeier-Haack Formylation / 6.1: |Suzuki-Miyaura Coupling;
DOI:10.1002/ejoc.201201339