3,3-difluorobutyl benzoate

Base Information

Chemical Name:3,3-difluorobutyl benzoate
CAS No.:569678-68-8
Molecular Formula:C₁₁H₁₂F₂O₂
Molecular Weight:214.212
Hs Code.:

Synonyms:3,3-difluorobutyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3-difluorobutyl benzoate

Chemical Property:

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Technology Process of 3,3-difluorobutyl benzoate

There total 2 articles about 3,3-difluorobutyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29342-27-6
3-oxobutyl benzoate

: 569678-68-8
3,3-difluorobutyl benzoate

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane;
DOI:10.1016/j.bmcl.2008.05.060

Reference yield:

: 98-88-4
benzoyl chloride

: 569678-68-8
3,3-difluorobutyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / dichloromethane / 1.5 h / -70 °C / Inert atmosphere

1.2: 17 h / -70 - 26 °C / Inert atmosphere

2.1: diethylamino-sulfur trifluoride / dichloromethane / 17 h / 0 - 26 °C / Inert atmosphere

With pyridine; diethylamino-sulfur trifluoride; In dichloromethane;