(3R,6S)-1-benzyl 3-methyl 6-(hydroxymethyl)piperidine-1,3-dicarboxylate

Base Information Edit

Chemical Name:(3R,6S)-1-benzyl 3-methyl 6-(hydroxymethyl)piperidine-1,3-dicarboxylate
CAS No.:1620675-51-5
Molecular Formula:C₁₆H₂₁NO₅
Molecular Weight:307.346
Hs Code.:
Mol file:1620675-51-5.mol

Synonyms:(3R,6S)-1-benzyl 3-methyl 6-(hydroxymethyl)piperidine-1,3-dicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,6S)-1-benzyl 3-methyl 6-(hydroxymethyl)piperidine-1,3-dicarboxylate Edit

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Technology Process of (3R,6S)-1-benzyl 3-methyl 6-(hydroxymethyl)piperidine-1,3-dicarboxylate

There total 10 articles about (3R,6S)-1-benzyl 3-methyl 6-(hydroxymethyl)piperidine-1,3-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56026-36-9
methyl 6-(hydroxymethyl)nicotinate

: 1620675-51-5
(3R,6S)-1-benzyl 3-methyl 6-(hydroxymethyl)piperidine-1,3-dicarboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: dmap; triethylamine / dichloromethane / 3 h / 20 °C

2: sodium cyanoborohydride; acetic acid / 4 h / 0 - 30 °C

3: tetrahydrofuran; water / 18 h / 20 °C

4: sodium hydrogencarbonate; potassium carbonate / methanol / 1 h / 20 °C

5: Chiraipak AD-Fl 25050mnmi.D,, / carbon dioxide; ethanol / 75007.5 Torr / Supercritical conditions; Resolution of racemate; liquid CO₂

With dmap; sodium cyanoborohydride; sodium hydrogencarbonate; potassium carbonate; acetic acid; triethylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; carbon dioxide; water;