1-(p-benzyloxy)cinnamoyl-2,4,6-tribenzyloxy-3,5-di-C-β-D-glucopyranosylbenzene

Base Information

Chemical Name:1-(p-benzyloxy)cinnamoyl-2,4,6-tribenzyloxy-3,5-di-C-β-D-glucopyranosylbenzene
CAS No.:897935-58-9
Molecular Formula:C₅₅H₅₆O₁₅
Molecular Weight:957.041
Hs Code.:

Synonyms:1-(p-benzyloxy)cinnamoyl-2,4,6-tribenzyloxy-3,5-di-C-β-D-glucopyranosylbenzene

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Chemical Property of 1-(p-benzyloxy)cinnamoyl-2,4,6-tribenzyloxy-3,5-di-C-β-D-glucopyranosylbenzene

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Technology Process of 1-(p-benzyloxy)cinnamoyl-2,4,6-tribenzyloxy-3,5-di-C-β-D-glucopyranosylbenzene

There total 3 articles about 1-(p-benzyloxy)cinnamoyl-2,4,6-tribenzyloxy-3,5-di-C-β-D-glucopyranosylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 897935-57-8
2,4,6-tri-O-benzyl-3,5-di-C-β-D-glucopyranosyl-phloroacetophenone

: 4397-53-9
p-benzyloxybenzaldehyde

: 897935-58-9
1-(p-benzyloxy)cinnamoyl-2,4,6-tribenzyloxy-3,5-di-C-β-D-glucopyranosylbenzene

Guidance literature:: With potassium hydroxide; In methanol; at 20 ℃; for 24h;
DOI:10.1016/j.carres.2006.02.019

Reference yield:

: 100-39-0
benzyl bromide

: 897935-58-9
1-(p-benzyloxy)cinnamoyl-2,4,6-tribenzyloxy-3,5-di-C-β-D-glucopyranosylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / K₂CO₃ / dimethylformamide / 20 °C

2: 84 percent / KOH / methanol / 24 h / 20 °C

With potassium hydroxide; potassium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2006.02.019

Reference yield:

: 160913-21-3
3',5'-di-C-β-D-glucosyl-2',4',6'-trihydroxyacetophenone

: 897935-58-9
1-(p-benzyloxy)cinnamoyl-2,4,6-tribenzyloxy-3,5-di-C-β-D-glucopyranosylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / K₂CO₃ / dimethylformamide / 20 °C

2: 84 percent / KOH / methanol / 24 h / 20 °C

With potassium hydroxide; potassium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2006.02.019