4-chlorostyryltrimethylsilane

Base Information

Chemical Name:4-chlorostyryltrimethylsilane
CAS No.:132536-25-5
Molecular Formula:C₁₁H₁₅ClSi
Molecular Weight:210.779
Hs Code.:

Synonyms:4-chlorostyryltrimethylsilane

Suppliers and Price of 4-chlorostyryltrimethylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chlorostyryltrimethylsilane

Chemical Property:

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Technology Process of 4-chlorostyryltrimethylsilane

There total 14 articles about 4-chlorostyryltrimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1073-67-2,24991-47-7
4-vinylbenzyl chloride

: 16029-98-4
trimethylsilyl iodide

: 88691-45-6,132536-25-5,88691-39-8
(E)-[2-(4-chlorophenyl)ethenyl]trimethylsilane

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; bis(3,5-di-tert-butylphenyl)(tert-butyl)phosphine; triethylamine; In 1,2-dichloro-ethane; at 40 ℃; for 24h; Inert atmosphere; Glovebox; Sealed tube;
DOI:10.1002/adsc.201500436

Reference yield: 92.0%

: 637-87-6
1-Chloro-4-iodobenzene

: 754-05-2
ethenyltrimethylsilane

: 88691-45-6,132536-25-5,88691-39-8
(E)-[2-(4-chlorophenyl)ethenyl]trimethylsilane

Guidance literature:: With palladium diacetate; 4 A molecular sieve; tetrabutylammonium acetate; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1016/S0040-4039(99)00062-3

Reference yield: 90.0%

: 5926-35-2
chlorobis(trimethylsilyl)methane

: 104-88-1
4-chlorobenzaldehyde

: 132536-25-5
4-chlorostyryltrimethylsilane

Guidance literature:: chlorobis(trimethylsilyl)methane; With sec.-butyllithium; In tetrahydrofuran; cyclohexane; at -78 ℃; for 0.666667h;

4-chlorobenzaldehyde; In tetrahydrofuran; cyclohexane; at -78 - 20 ℃; Further stages.;
DOI:10.1039/b716897g