C₂H₅C(O)Os(CO)4Re(CO)5

Base Information

Chemical Name:C₂H₅C(O)Os(CO)4Re(CO)5
CAS No.:98688-95-0
Molecular Formula:C₁₂H₅O₁₀OsRe
Molecular Weight:685.573
Hs Code.:

C<sub>2</sub>H<sub>5</sub>C(O)Os(CO)4Re(CO)5

Synonyms:C₂H₅C(O)Os(CO)4Re(CO)5

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂H₅C(O)Os(CO)4Re(CO)5

Chemical Property:

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Technology Process of C₂H₅C(O)Os(CO)4Re(CO)5

There total 2 articles about C₂H₅C(O)Os(CO)4Re(CO)5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 16457-30-0
hydridopentacarbonylrhenium(I)

: (CO)4Os(CH₂CH₃)2

: 98688-96-1
C₂H₅Os(CO)4Re(CO)5

: 98688-95-0
C₂H₅C(O)Os(CO)4Re(CO)5

: 98688-92-7
Re₂Os*13CO*C⁽²⁾H₃CN=Re₂Os(CO)13(C⁽²⁾H₃CN)

: 123-38-6
propionaldehyde

Guidance literature:: With CH₃CN; In acetonitrile; byproducts: C2H6; Et2Os(CO)4 and HRe(CO)5 (1:1 molar ratio) were heated in MeCN to 45°C for 20 h; solvent was removed, residue was placed under high vac. overnight and subjected to preparative layer chromy.; elem. anal. for EtOsRe(CO)9;

Reference yield:

: 16457-30-0
hydridopentacarbonylrhenium(I)

: (CO)4Os(CH₂CH₃)2

: 2206-26-0
[D₃]acetonitrile

: 98688-95-0
C₂H₅C(O)Os(CO)4Re(CO)5

: 98688-94-9
C₂H₅C(O)Os(CO)3(C⁽²⁾H₃CN)Re(CO)5

: 123-38-6
propionaldehyde

Guidance literature:: In [D₃]acetonitrile; byproducts: C2H6; Et2Os(CO)4, HRe(CO)5 (1 equiv), and CD3CN were sealed under vac. in an NMR tube, reaction was heated to 49°C for 25 h; the tube was broken open on the vac. line and the volatiles distilled into an NMR tube, the (1)H NMR spectrum showed that EtH/EtCHO ratio was 4.2,;