N^α-(o-nitrophenylsulfenyl)-N^ε-(trifluoroacetyl)-L-lysine N-hydroxysuccinimide ester

Base Information

• Chemical Name: N^α-(o-nitrophenylsulfenyl)-N^ε-(trifluoroacetyl)-L-lysine N-hydroxysuccinimide ester
• CAS No.: 64851-79-2
• Molecular Formula: C₁₈H₁₉F₃N₄O₇S
• Molecular Weight: 492.433

Synonyms:N^α-(o-nitrophenylsulfenyl)-N^ε-(trifluoroacetyl)-L-lysine N-hydroxysuccinimide ester

Chemical Property of N^α-(o-nitrophenylsulfenyl)-N^ε-(trifluoroacetyl)-L-lysine N-hydroxysuccinimide ester

Chemical Property:

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Technology Process of N^α-(o-nitrophenylsulfenyl)-N^ε-(trifluoroacetyl)-L-lysine N-hydroxysuccinimide ester

There total 3 articles about N^α-(o-nitrophenylsulfenyl)-N^ε-(trifluoroacetyl)-L-lysine N-hydroxysuccinimide ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-hydroxy-pyrrolidine-2,5-dione (6066-82-6) + Nα-(o-nitrophenylsulfenyl)-Nε-(trifluoroacetyl)lysine (41918-63-2) → Nα-(o-nitrophenylsulfenyl)-Nε-(trifluoroacetyl)-L-lysine N-hydroxysuccinimide ester (64851-79-2)

Guidance literature:

With dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane; at 0 - 20 ℃; for 7h;

Reference yield:

(S)-6-trifluoroacetylamino-2-aminohexanoic acid (10009-20-8,96193-68-9) → Nα-(o-nitrophenylsulfenyl)-Nε-(trifluoroacetyl)-L-lysine N-hydroxysuccinimide ester (64851-79-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 2N NaOH / acetone

2: dicyclohexylcarbodiimide / dioxane; CH₂Cl₂ / 7 h / 0 - 20 °C

With sodium hydroxide; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane; acetone;

Reference yield:

2-nitrobenzenesulfenyl chloride (7669-54-7) → Nα-(o-nitrophenylsulfenyl)-Nε-(trifluoroacetyl)-L-lysine N-hydroxysuccinimide ester (64851-79-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 2N NaOH / acetone

2: dicyclohexylcarbodiimide / dioxane; CH₂Cl₂ / 7 h / 0 - 20 °C

With sodium hydroxide; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane; acetone;

upstream raw materials:

1-hydroxy-pyrrolidine-2,5-dione

N^α-(o-nitrophenylsulfenyl)-N^ε-(trifluoroacetyl)lysine

(S)-6-trifluoroacetylamino-2-aminohexanoic acid

2-nitrobenzenesulfenyl chloride

Downstream raw materials:

N^α-(o-nitrophenylsulfenyl)-N^ε-(trifluoroacetyl)-L-lysyl-L-alanyl-L-alanine methyl ester

N^α-(o-nitrophenylsulfenyl)-N^ε-(trifluoroacetyl)-L-lysyl-L-leucine methyl ester

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