Phenyl-(2,3-di-O-benzyl-6-desoxy-D-xylo-hexopyranos-4-ulosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

Base Information

Chemical Name:Phenyl-(2,3-di-O-benzyl-6-desoxy-D-xylo-hexopyranos-4-ulosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid
CAS No.:96701-98-3
Molecular Formula:C₅₃H₅₄O₁₀
Molecular Weight:851.006
Hs Code.:

Synonyms:Phenyl-(2,3-di-O-benzyl-6-desoxy-D-xylo-hexopyranos-4-ulosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

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Chemical Property of Phenyl-(2,3-di-O-benzyl-6-desoxy-D-xylo-hexopyranos-4-ulosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

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Technology Process of Phenyl-(2,3-di-O-benzyl-6-desoxy-D-xylo-hexopyranos-4-ulosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

There total 1 articles about Phenyl-(2,3-di-O-benzyl-6-desoxy-D-xylo-hexopyranos-4-ulosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 87591-22-8
Phenyl-O-<2,3-di-O-benzyl-6-desoxy-α-D-glucopyranosyl>-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

: 96701-98-3
Phenyl-(2,3-di-O-benzyl-6-desoxy-D-xylo-hexopyranos-4-ulosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

Guidance literature:: With acetic anhydride; In dimethyl sulfoxide; for 72h; Ambient temperature;

Reference yield: 70.0%

: 96701-98-3
Phenyl-(2,3-di-O-benzyl-6-desoxy-D-xylo-hexopyranos-4-ulosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

: 96701-99-4,96745-48-1
Phenyl-(2,3-di-O-benzyl-4,6-didesoxy-4-hydroxyimino-D-xylo-hexopyranos-4-ulosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In ethanol; dichloromethane; at 40 ℃; for 2h;

Reference yield:

: 96701-98-3
Phenyl-(2,3-di-O-benzyl-6-desoxy-D-xylo-hexopyranos-4-ulosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

: 96702-01-1
Phenyl-<(4S)-2,3-di-O-benzyl-4,6-didesoxy-4-(2,2-dimethyl-1,3-dioxolan-4-ylmethyl)amino-α-D-galactopyranosyl>-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / hydroxylamine-hydrochloride, NaOAc / CH₂Cl₂; ethanol / 2 h / 40 °C

2: 68 percent / LiAlH₄ / diethyl ether / 3 h

3: 69 percent / molecular sieve, NaCNBH₃, glacial acetic acid / methanol / 2 h / Ambient temperature

With lithium aluminium tetrahydride; molecular sieve; hydroxylamine hydrochloride; sodium acetate; sodium cyanoborohydride; acetic acid; In methanol; diethyl ether; ethanol; dichloromethane;