1-[Bis(trimethylsiloxy)phosphinoyl]-1-[2-(2,2,3,3-tetrafluoropropoxytrimethylsiloxyphosphinoyl)phenyl]hexafluoroisobutene

Base Information

• Chemical Name: 1-[Bis(trimethylsiloxy)phosphinoyl]-1-[2-(2,2,3,3-tetrafluoropropoxytrimethylsiloxyphosphinoyl)phenyl]hexafluoroisobutene
• CAS No.: 137789-97-0
• Molecular Formula: C₂₂H₃₄F₁₀O₈P₂Si₃
• Molecular Weight: 762.695

Synonyms:1-[Bis(trimethylsiloxy)phosphinoyl]-1-[2-(2,2,3,3-tetrafluoropropoxytrimethylsiloxyphosphinoyl)phenyl]hexafluoroisobutene

Chemical Property of 1-[Bis(trimethylsiloxy)phosphinoyl]-1-[2-(2,2,3,3-tetrafluoropropoxytrimethylsiloxyphosphinoyl)phenyl]hexafluoroisobutene

Chemical Property:

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Technology Process of 1-[Bis(trimethylsiloxy)phosphinoyl]-1-[2-(2,2,3,3-tetrafluoropropoxytrimethylsiloxyphosphinoyl)phenyl]hexafluoroisobutene

There total 2 articles about 1-[Bis(trimethylsiloxy)phosphinoyl]-1-[2-(2,2,3,3-tetrafluoropropoxytrimethylsiloxyphosphinoyl)phenyl]hexafluoroisobutene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tris(trimethylsilyl) phosphite (1795-31-9) + 6-Oxo-6-(2,2,3,3-tetrafluoro-propoxy)-8,8-bis-trifluoromethyl-5,7-dioxa-6λ5-phospha-benzocyclohepten-9-one (137789-96-9) → 1-[Bis(trimethylsiloxy)phosphinoyl]-1-[2-(2,2,3,3-tetrafluoropropoxytrimethylsiloxyphosphinoyl)phenyl]hexafluoroisobutene (137789-97-0)

Guidance literature:

at 5 - 10 ℃;

Reference yield:

2-(2,2,3,3-tetrafluoropropoxy)benzo[e][1,3,2]dioxaphosphinin-4-one (137073-23-5) → 1-[Bis(trimethylsiloxy)phosphinoyl]-1-[2-(2,2,3,3-tetrafluoropropoxytrimethylsiloxyphosphinoyl)phenyl]hexafluoroisobutene (137789-97-0)

Guidance literature:

DOI:10.1016/S0022-1139(00)83808-7

Reference yield: 61.0%

1-[Bis(trimethylsiloxy)phosphinoyl]-1-[2-(2,2,3,3-tetrafluoropropoxytrimethylsiloxyphosphinoyl)phenyl]hexafluoroisobutene (137789-97-0) → 3,3,3-trifluoro-1-(2-hydroxyphenyl)-2-trifluoromethylpropan-1-one

Guidance literature:

With water; In ethanol; for 3h; Heating;

upstream raw materials:

tris(trimethylsilyl) phosphite

6-Oxo-6-(2,2,3,3-tetrafluoro-propoxy)-8,8-bis-trifluoromethyl-5,7-dioxa-6λ⁵-phospha-benzocyclohepten-9-one

2-(2,2,3,3-tetrafluoropropoxy)benzo[e][1,3,2]dioxaphosphinin-4-one

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