tris[2-butyloxy-3-methyl-5-(N'-(4-nitrophenyl)ureido)benzyl]phosphine oxide

Base Information

Chemical Name:tris[2-butyloxy-3-methyl-5-(N'-(4-nitrophenyl)ureido)benzyl]phosphine oxide
CAS No.:1383275-05-5
Molecular Formula:C₅₇H₆₆N₉O₁₃P
Molecular Weight:1116.18
Hs Code.:

Synonyms:tris[2-butyloxy-3-methyl-5-(N'-(4-nitrophenyl)ureido)benzyl]phosphine oxide

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Chemical Property of tris[2-butyloxy-3-methyl-5-(N'-(4-nitrophenyl)ureido)benzyl]phosphine oxide

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Technology Process of tris[2-butyloxy-3-methyl-5-(N'-(4-nitrophenyl)ureido)benzyl]phosphine oxide

There total 2 articles about tris[2-butyloxy-3-methyl-5-(N'-(4-nitrophenyl)ureido)benzyl]phosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1169880-48-1
tris(2-butyloxy-3-methyl-5-aminobenzyl)phosphine oxide

: 100-28-7
4-Nitrophenyl isocyanate

: 1383275-05-5
tris[2-butyloxy-3-methyl-5-(N'-(4-nitrophenyl)ureido)benzyl]phosphine oxide

Guidance literature:: In dichloromethane; at 20 ℃;
DOI:10.1016/j.tetlet.2012.05.018

Reference yield:

: 1245080-97-0
C₃₆H₄₈N₃O₁₀P

: 1383275-05-5
tris[2-butyloxy-3-methyl-5-(N'-(4-nitrophenyl)ureido)benzyl]phosphine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / 6 h / Reflux

2: dichloromethane / 20 °C

With hydrazine hydrate; In methanol; dichloromethane;
DOI:10.1016/j.tetlet.2012.05.018