p-acetamidophenyl methyl disulfide

Base Information

• Chemical Name: p-acetamidophenyl methyl disulfide
• CAS No.: 1042696-72-9
• Molecular Formula: C₉H₁₁NOS₂
• Molecular Weight: 213.324
• Mol file: 1042696-72-9.mol

Synonyms:p-acetamidophenyl methyl disulfide

Chemical Property of p-acetamidophenyl methyl disulfide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of p-acetamidophenyl methyl disulfide

There total 2 articles about p-acetamidophenyl methyl disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

4-methyldisulfanyl-phenylamine (1042696-70-7) + acetyl chloride (75-36-5) → p-acetamidophenyl methyl disulfide (1042696-72-9)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1016/j.bmc.2008.05.032

Reference yield:

4-aminotiophenol (1193-02-8) → p-acetamidophenyl methyl disulfide (1042696-72-9)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol / 2 h / 20 °C

2: triethylamine / dichloromethane / 1 h / 20 °C

With triethylamine; In methanol; dichloromethane;

upstream raw materials:

4-methyldisulfanyl-phenylamine

acetyl chloride

4-aminotiophenol